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机构地区:[1]黑龙江省科学院高技术研究院,黑龙江哈尔滨150040
出 处:《化学与粘合》2016年第3期191-193,共3页Chemistry and Adhesion
基 金:哈尔滨市科技局创新人才基金项目;(编号:RC2009QD018003)
摘 要:以椰子油酸单乙醇酰胺、环氧丁烷为原料,进行开环聚合反应合成椰子油酸单乙醇酰胺丁氧基醚,考察了椰子油酸单乙醇酰胺丁氧基醚合成的条件。实验表明,在反应物椰子油酸单乙醇酰胺与环氧丁烷物质的量比为1∶2,反应温度155℃,反应时间3h的条件下,环氧丁烷的转化率可达98.0%以上。The coconut oil monoethanolamide butoxy ether was prepared from coconut oil monoethanolamide and epoxybutane by the ring-open- ing polymerization method. The reaction conditions for the synthesis of coconut oil monoethanolamide butoxy ether were investigated. The optimum re- action conditions were obtained as follows: the molar ratio of coconut oil monoethanolamide to epoxybutane was 1:2,the reaction temperature and time was 155℃ and 3h respectively. Under these conditions, the conversion of epoxybutane was 98.0%.
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