卷烟侧流烟气中氨释放量的连续流动法测定  

Determination of ammonia in sidestream cigarette smoke by continuous flow analysis method

作　　者：王洪波[1] 郭军伟[1] 殷延齐[2] 刘绍锋[1] 赵晓东[1] 谢复炜[1] 赵乐[1] 

机构地区：[1]中国烟草总公司郑州烟草研究院 [2]江苏中烟工业有限责任公司徐州卷烟厂,江苏省徐州市环城路80号221000

出　　处：《烟草科技》2016年第5期38-44,共7页Tobacco Science & Technology

基　　金：中国烟草总公司标准预研项目"卷烟侧流烟气中氨的测定"(2014QB012)

摘　　要：建立了利用连续流动分析仪测定卷烟侧流烟气中氨释放量的分析方法。采用鱼尾罩、剑桥滤片和盛有稀盐酸的吸收瓶捕集卷烟侧流烟气中的氨,经处理后用连续流动分析仪测定。结果表明：1方法的线性关系良好（相关系数为0.999 9）,检出限为0.12 mg/支,RSD≤6.8%（n=5）,加标回收率在86.0%-112.0%之间;2该方法简便、快速、准确,适用于卷烟侧流烟气中氨释放量的测定。An analytical method for quantifying ammonia in sidestream cigarette smoke（SCS）was developed with continuous flow analysis. Ammonia in SCS was collected by a＂fishtail＂chimney, by passing through a Cambridge filter pad and an absorption bottle containing hydrochloric acid. The combined collection was subjected to washing and extraction before being analyzed by a continuous flow method. The results showed that： 1）The method had good linearity（with correlation coefficient of 0.999 9）and the limit of detection was0.12 mg/cig. The relative standard deviation was 6.8%（n=5）, and the recoveries ranged from 86.0% to 112.0%.2）The method was simple, rapid, accurate, and suitable for determining the level of ammonia in SCS.

关 键 词：卷烟 侧流烟气 氨 连续流动法 

分 类 号：TS411.2[农业科学—烟草工业]