制备过氧化钙的新方法研究  

Study on the New Method of Preparing Calcium Peroxide

作　　者：蒋军泽 赵鑫[1] 穆瑞珠[1] 刘建萍 李原芳[1] 胡小莉[1] 

机构地区：[1]西南大学化学化工学院,重庆400715 [2]重庆第48中学,重庆400700

出　　处：《西南师范大学学报（自然科学版）》2016年第7期177-180,共4页Journal of Southwest China Normal University(Natural Science Edition)

摘　　要：针对大学本科"过氧化钙的制备及含量测定"实验中存在的耗时长、产率低和氨水污染等问题,采用CaCl2和H2O2为主要原料,以NaOH溶液代替氨水作为反应介质,对试剂浓度、反应温度、加料顺序等各种影响因素进行了深入研究,从而总结出最佳实验条件,制备出产率高、纯度好、性能稳定的产品,为"无机制备"课程开设该实验提供了一套成功率高、效果好的实验方案.T his article is aimed at the experim ent^ problem of The Preparation and Content Determinationo f Calcium Peroxide for college undergraduate, which has disadvantages like long tim e consum ing, lowyield and the pollution of anm onia w ater etc. Calcium chloride and hydrogen peroxide w ere used as them ain reaction reagents. Sodium hydroxide, replaced am m onia w ater, w as adopted as reaction m edium inthe laboratory. All the influential factors w ere studied by the m ono-factor experim ents, such as reagentconcentration, reaction tem perature and reagent addition order. T he m ethod w as prepared w ith high yield,good purity, stable perform ance of p ro d ucts; w hich provided the course Inorganic P reparation w ith a reliableand effective scheme.

关 键 词：过氧化钙 氢氧化钠 制备 

分 类 号：O614.23[理学—无机化学] O631[理学—化学]