前列腺炎丸的质量标准研究  

Quality Standard for Prostatitis Pills

作　　者：陈玉铭[1] 张琦[1] 韩丹[1] 刘丹[1] 赵庆兰[1] 

机构地区：[1]解放军208医院药剂科,吉林长春130062

出　　处：《解放军药学学报》2016年第3期246-248,共3页Pharmaceutical Journal of Chinese People's Liberation Army

摘　　要：目的建立前列腺炎丸质量标准。方法采用HPLC法对黄柏中盐酸小檗碱进行含量测定;同时对其中的王不留行、黄柏、薏苡仁进行TLC鉴别。结果 HPLC法测定盐酸小檗碱在2.5～100μg·ml-1（r=0.9998）范围内与峰面积有良好的线性关系,平均加样回收率为100.5%。同时TLC检出了王不留行、黄柏、薏苡仁的特征斑点。结论该方法重复性好、简便、稳定性好,能够有效控制前列腺炎丸的质量。Objective To establish a quality standard for prostatitis pills. Methods HPLC method was used for content determination of berberine hydrochloride in cortex phellodendri. Cowherd seed line, cortex phellodendri, and eoix seed were identified by TLC. Results Berberine hydrochloride within the range of 2.5 - 100 μg .ml-1 （r = 0.9998） showed a good linear relationship with the peak area. The average recovery was 100.5%. TLC detected cowherb seed, cortex phellodendri and semen coicis. Conclusion This method is repeatable, simple and stable, which can effectively control the quality of prostatitis pills.

关 键 词：前列腺炎丸 HPLC TLC 质量标准 

分 类 号：R917[医药卫生—药物分析学]