复方蜂胶胶囊中非法添加格列波脲的分离与鉴定  

Isolation and Identification of Glibornuride Illegally Added in Compound Propolis Capsules

作　　者：黄海燕[1] 钟建理[1] 饶伟文[1] 陈瀚[1] 

机构地区：[1]广西壮族自治区桂林食品药品检验所,广西桂林541002

出　　处：《中国药业》2016年第14期76-78,共3页China Pharmaceuticals

摘　　要：目的分离和鉴定复方蜂胶胶囊中非法添加的格列波脲。方法采用半制备液相色谱法分离该化合物,并用波谱法鉴定其结构。结果从复方蜂胶胶囊中分离纯化得到的化合物,经核磁共振(NMR)验证了其结构。结论复方蜂胶胶囊中非法添加组分为格列波脲。Objective To separate and identify the structure of the glibornuride as an illegal adulterant in a health product Compound Propolis capsules. Methods A pectroscopic method was used to isolate and a NMR method was used to identify the structure of glibornuride. Results The chemical structure of the compound isolated from the capsule was identified by NMR. Conclusion The compound is glibornuride,which is illegally added in Compound Propolis Capsules.

关 键 词：复方蜂胶胶囊 格列波脲 分离 鉴定 核磁共振 

分 类 号：R954[医药卫生—药学] R284.1