行业标准方法测试口含烟化学指标的适用性  

Suitability of industrial standard methods in testing chemical constituents of oral tobacco products

作　　者：李鹏[1] 王申 张东豫 袁大林 刘剑 代远刚 陈森林[7] 沈轶 LI Peng WANG Shen ZHANG Dongyu YUAN Dalin LIU Jian DAI Yuangang CHEN Senlin SHEN Yi(Zhengzhou Tobacco Research Institute of CNTC, Zhengzhou 450001, China Shanghai New Type Tobacco Product Research Institute, Shanghai 200082, China China Tobacco Henan Industrial Co., Ltd., Zhengzhou 450000, China China Tobacco Yunnan Industrial Co., Ltd., Kunming 653100, China China Tobacco Guizhou Industrial Co., Ltd., Guiyang 550001, China China Tobacco Hunan Industrial Co., Ltd., Changsha 410016, China China Tobacco Guangdong Industrial Co., Ltd., Guangzhou 510385, China)

机构地区：[1]中国烟草总公司郑州烟草研究院 [2]上海新型烟草制品研究院,上海市虹桥区大连路789号200082 [3]河南中烟工业有限责任公司,郑州市管城区陇海东路72号450000 [4]云南中烟工业有限责任公司,昆明市盘龙区世博路6号653100 [5]贵州中烟工业有限责任公司,贵阳市云岩区友谊路25号550001 [6]湖南中烟工业有限责任公司 [7]广东中烟工业有限责任公司

出　　处：《烟草科技》2016年第9期57-62,共6页Tobacco Science & Technology

基　　金：中国烟草总公司标准项目"口含烟质量安全卫生标准研究"(中烟办[2014]48号);"口含烟产品标准研究"(中烟办[2014]214号)

摘　　要：为研究现行的行业标准方法对口含烟样品化学指标的适用性,以企业自制口含烟为样本,在行业内7家实验室开展了烟碱、含水率、pH、甘油、1,2-丙二醇、重金属、TSNAs等指标的共同实验。结果表明：①针对烟碱、含水率、pH、甘油、1,2-丙二醇、重金属、TSNAs等指标,现行行业标准检测方法的重复性标准偏差与均值的比值范围为0.20%～7.20%,再现性标准偏差与均值的比值范围为1.56%～32.28%。②现行的行业标准检测方法的前处理技术以及色谱检测条件均适用于口含烟样品。但称量袋装口含烟时,需先用剪刀将样品从中间剪开,无需过筛,小袋计入样品总质量。③袋装口含烟含水率普遍较高,因此可以根据样品情况适当调节称取质量和萃取溶剂体积。To evaluate the suitability of current industrial standard methods in determining the contents of nicotine, moisture, glycerol, 1,2-propylene glycol, heavy metals, TSNAs and pH of oral tobacco products, collaborative studies were carried out by seven laboratories. The results showed that： 1） For the chemical indexes mentioned above, the ratio of repeatability standard deviation （St） to the mean value ranged from 0.20% to 7.20% and the ratio of reproducibility standard deviation （SR） to the mean value was from 1.56% to 32.28%. 2） The sample treatments and chromatography conditions of the current detection methods were suitable to analyze these constituents in oral tobacco products. However, the samples of pouched oral tobacco products must be cut into two parts （e.g., by using scissors） before they were weighed, and the weight of pouch was accounted into the total weight of the sample. 3） Considering the higher moisture content in pouched oral tobacco products, sample weight and extraction solvent volume should be adjusted according to the moisture content in samples.

关 键 词：口含烟 烟碱 含水率 PH 甘油 1 2-丙二醇 重金属 TSNA 共同实验 

分 类 号：TS411.1[农业科学—烟草工业]