反应合成Ti-Sn微米棒  

Fabrication of Ti-Sn Micro-rod by Reaction Synthesis

作　　者：梁宝岩[1] 张旺玺[1] 王艳芝[1] 徐世帅[1] 王俊和[1] 闫帅帅[1] LIANG Baoyan ZHANG Wangxi WANG Yanzhi XU Shishuai WANG Junhe YAN Shuaishua(School of Materials and Chemical Engineering Zhongyuan University of Technology, Zhengzhou 450007, Chin)

机构地区：[1]中原工学院材料与化工学院,郑州450007

出　　处：《中国陶瓷》2016年第9期65-68,共4页China Ceramics

基　　金：郑州市国际科技合作与交流项目(153PGJHZ209);河南省教育厅重点项目(13A430132;151RTSTHN004);河南省教育厅自然科学研究计划项目资助(12A430024;13A430128;14A430007);河南省基础与前沿技术研究计划(132300410164);河南省省院科技合作项目(122106000051;142106000193);河南省科技开放合作项目(142106000051);郑州市人才引育项目(141PRCYY514)

摘　　要：采用微波热处理技术得到了Ti-Sn微米棒。采用XRD、SEM与EDS研究合成产物的组成相组成和微观形貌。研究结果表明,通过微波合成技术,采用2Ti/Sn/石墨粉体原料均得到大量Ti Sn微米棒。Ti-Sn微米棒的长度约5~10μm,宽度约2~3μm。石墨原料起到了诱发电弧放电的作用,从而促进Ti Sn柱状晶的形成。The Ti-Sn micro-rod was synthesized by microwave heat treatment. The phase composition and microstructure of the samples were studied by XRD, SEM and EDS. The result showed that amounts of Ti-Sn microrods can be obtained by microwave synthesis from 2Ti/Sn/graphite. These micro-rods had a length of 5 ~ 10 μm and a width of 2 ~ 3 μm. Graphite played a role for inducing arc discharge and was benefits to synthesis of Ti-Sn micro-rod.

关 键 词：Ti-Sn微米棒 微波合成技术 

分 类 号：TQ174.758.12[化学工程—陶瓷工业]