Hastelloy C-276合金Σ3晶界和Σ9晶界随着退火时间的演变规律（英文）  

Influence of Annealing Time on Σ3 Boundary and Σ9 Boundary Evolutions in Hastelloy C-276 Alloy

作　　者：张晓宇[1,2] 李德富[1] 郭胜利[1] 赵宪明[2] 

机构地区：[1]北京有色金属研究总院,北京100088 [2]东北大学轧制技术及连轧自动化国家重点实验室,辽宁沈阳110004

出　　处：《稀有金属材料与工程》2016年第9期2253-2257,共5页Rare Metal Materials and Engineering

基　　金：National Natural Science Foundation of China(50834008)

摘　　要：Hastelloy C-276合金经小变形量冷轧后进行1100℃不同时间的退火处理。采用EBSD技术对Σ3和Σ9晶界比例进行统计,同时采用五参数法对Σ3和Σ9晶界面分布进行分析。结果表明,Σ3晶界随着退火时间的延长更加接近于标准重合点阵晶界取向,而其晶界面更加接近于低能量的{111}晶界面。这一结果符合晶界"微调"机制。Σ9晶界面分布则越来越集中在[110]晶带。而偏差较大的Σ9晶界比例增加,是由于非共格Σ3比例的增加导致的。Hastelloy C-276 was subjected to low strain deformation and then annealed at 1100 ℃ for different time. The Σ3 and Σ9 boundary percentages and grain boundary plane distributions were characterized by electron back-scatter diffraction（EBSD） and a five-parameter analysis method. The results show that the Σ3 boundary evolves towards a more exact coincident-site lattice（CSL） misorientation and the Σ3 boundary plane is closer to low surface energy plane {111} with the increasing of annealing time. This is consistent with fine tuning mechanism. While the population of incoherent Σ3 boundary is increasing, the proportion of Σ9 boundary with larger deviations increase, too. And the distributions of grain boundary density planes for Σ9 boundary are more intensive on the whole [110] zone.

关 键 词：HASTELLOY C-276合金 Σ3和Σ9晶界 晶界面分布 EBSD 

分 类 号：TG156.2[金属学及工艺—热处理] TG146.15[金属学及工艺—金属学]