溶剂热合成法制备(Zn,Hg)S微晶和薄膜  

Preparation of (Zn,Hg)S Crystallite and Thin Film by Solvothermal Synthesis

作　　者：李雪梅[1] 杨延钊[1] 孙思修[1] 郭今心[1] 钟红梅[1] 李大枝[1] 

机构地区：[1]山东大学化学与化工学院,济南250100

出　　处：《无机化学学报》2002年第9期961-964,共4页Chinese Journal of Inorganic Chemistry

基　　金：国家自然科学基金资助项目(No.20171029);山东省优秀中青年科学家科研奖励基金。

摘　　要：The crystallite and thin film of (Zn,Hg)S at different solvents were prepared by thermolysis of thiocyanoto complexes. The samples were characterized by X ray diffraction (XRD), transmission electron microscopy (TEM) and scanning electron microscopy (SEM). The results of these studies show that the properties of solvents are important in controlling the sizes and shapes of the final products.The crystallite and thin film of (Zn,Hg)S at different solvents were prepared by thermolysis of thiocyanoto complexes. The samples were characterized by X ray diffraction (XRD), transmission electron microscopy (TEM) and scanning electron microscopy (SEM). The results of these studies show that the properties of solvents are important in controlling the sizes and shapes of the final products.

关 键 词：溶剂热合成法 制备 硫化物 微晶 薄膜 硫化锌 硫化汞 半导体材料 

分 类 号：TN304.25[电子电信—物理电子学]