苏格木勒-3汤中白豆蔻-白苣胜挥发油部位体外GC-MS分析  

The Analysis of Essential oil of Baidoukou-Baijusheng of Sugmel-3 in Vitro by GC-MS

作　　者：敖道夫[1] 呼日乐巴根[2] 阿拉坦敖日格乐[2] 萨础拉[2] 

机构地区：[1]内蒙古民族大学附属医院,内蒙古通辽028000 [2]内蒙古医科大学,内蒙古呼和浩特010110

出　　处：《中医药导报》2016年第24期41-42,46,共3页Guiding Journal of Traditional Chinese Medicine and Pharmacy

基　　金：内蒙古医科大学博士启动基金项目(No.BSJJ2013QNCX016);内蒙古医科大学青年创新基金项目(No.YKD2013QNCX016)

摘　　要：目的:建立苏格木勒-3汤中白豆蔻-白苣胜挥发油部位体外GC-MS图谱,分析其体外化学成分。方法:水蒸气蒸馏法提取苏格木勒-3汤中白豆蔻-白苣胜挥发油部位,采用气相色谱-质谱联用方法(GC-MS)分析其化学成分及相对含量。结果:从白豆蔻-白苣胜挥发油各色谱峰中共鉴定出59个种化学成分,其中"表观丰度"最大的为10号峰桉油精(73.73%),2、5号α-蒎烯(2.30%、9.96%)、23号α-松油醇(6.46%)、4号峰α-水芹烯(1.00%)、6号峰α-月桂烯(0.82%)、12号峰γ-萜品烯(0.81%)、15号峰β-芳樟醇(0.72%)7个成分为白豆蔻-白苣胜挥发油中主要特征性成分。结论:苏格木勒-3汤中白豆蔻-白苣胜挥发油部位是主要药效组分,且分析得到的成分均为本方有效物质基础;建立的方法可作为本方挥发性成分的质量控制方法。Objective： To establish the GC-MS chromatograms of essential oil of Baidoukou-Baijusheng of Sugmel-3 in vitro, analyze and identify its chemical component. Methods： The essential oil of Baidoukou-Bai- jusheng of Sugmel-3 was extracted by steam distillation and analyzed chemical component and relative amount by GC-MS technique. Results： 59 constituents were identified from Baidoukou-Baijusheng essential oil. The greatest for ＂apparent abundance＂ was a 10 peak eucalyptol. The major constituents were 2,5 peak α-pinene （2.30%, 9.96%）, 23 peak α-terpineol （6.46%）, 4 peak α-pheltandrene （1.00%）, 6 peak α-myrcene （0.82%）, 12 peakγ-terpinene （0.81%）, 15 peak β-linalool （0.72%）. The major constituents for 7 were the main characteristic components for Baidoukou-Baijusheng essential oil. Conclusion： The Baidoukou-Baijusheng essential oil of Sugmel-3 were the primary efficacy components and this characteristic components was the effective material basis of Sugmel-3; The established method can be used for quality control of essential oil of Sugmel-3.

关 键 词：苏格木勒-3汤 白豆蔻-白苣胜挥发油 化学成分 气相色谱-质谱联用法 

分 类 号：R284[医药卫生—中药学]