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作 者:吴梦一[1]
出 处:《低温与特气》2017年第1期33-36,共4页Low Temperature and Specialty Gases
基 金:中国安全生产科学研究院基本科研业务专项资金(2015JBKY08)
摘 要:介绍了溶剂解吸—气相色谱法测定工作场所空气中丙酮测量不确定度的评定过程,确定了不确定度分量的来源及大小。其中活性炭解吸液中丙酮的浓度和标准采样体积的贡献较大。可优先选择高精密度的仪器和实验器具,同时不断提高人员操作水平,有效降低不确定度。In this paper, the uncertainty evaluation process of determination of acetone in the air of workplace by solvent desorption-gas chromatography was introduced, and it determined the source and value of the uncertainty. The concentra- tion of acetone in the desorption solution of the activated carbon and the standard sampling volume made the greater contri- bution. In order to reduce the uncertainty effectively, high-precision instruments and experimental apparatus should be given priority. At the same time, the level of personnel operations should be improved continuously.
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