泰国甲仑榴莲的果肉及内果皮挥发油成分的GC-MS分析  

Analysis of Essential Oil in Pulp and Peel of Thailand Jialun Durian by GC/MS

作　　者：刘玉峰[1] 王志萍[1] 胡延喜[1] 韩彬[2] 王彦军 刘景凡 卢晓丹 

机构地区：[1]辽宁大学药学院,辽宁沈阳110036 [2]黑龙江中医药大学药学院,黑龙江哈尔滨150040 [3]河北美威药业股份有限公司,河北安国310051 [4]沈阳市120中学化学组,辽宁沈阳110036

出　　处：《辽宁大学学报（自然科学版）》2017年第1期41-44,共4页Journal of Liaoning University：Natural Sciences Edition

基　　金：国家自然科学基金青年项目(81403177);沈阳市科技局应用基础项目(F12-277-1-14)

摘　　要：目的:分析甲仑榴莲挥发油成分,为开发利用榴莲资源和质量控制提供科学依据.方法:采用水蒸气蒸馏法提取榴莲果肉及内果皮中的挥发油,采用GC-MS法和NIST98谱图库鉴定化学成分.结果:从榴莲果肉中鉴定出11种化合物,其含量占挥发油总含量的98.86%,其主要成分及相对含量分别为环十六烷(43.59%),9-十六碳烯酸乙酯(11.17%),十六烷(10.59%),棕榈酸乙酯(9.12%),以烷类和酯类化合物为主;从榴莲内果皮中鉴定出11种化合物,占总挥发油含量的95.73%,其主要成分及相对含量分别为十六烷(25.71%),2-十四烯(E)(22.41%),9-十六碳烯酸乙酯(13.56%),苯乙烯(13.45%),以烷类和烯烃类为主.结论:为榴莲挥发油的进一步研究及开发利用提供科学依据.Objective： To analyze the constituents of the essential oils extracted from Jia Lun durian,and provide scientific basis for quality control of it. Methods： The essential oils were extracted from durian pulp and peel by water steam distillation. The components were identified by GC-M S and NIST data base. Results： 11 compounds from durian pulp were identified and accounted for 98. 86% of all essential oil. The main components were hexadecane（ 43. 59%）,ethyl 9-hexadecenoate（ 11. 17%）,hexadecane（ 10. 59%）,palmitic acid ethyl ester（ 9. 12%）.Alkanes and esters were the main components. In durian peel,the 11 kinds of compounds wereidentified and accounted for 95. 73% of the total volatile oil,in which was mainly hexadecane（ 25. 71%）,2-tetradecene（ E）（ 22. 41%）,ethyl 9-hexadecenoate（ 13. 56%）,styrene（ 13. 45%）.Alkanes and alkene were the main components. Conclusion： The study provided a scientific basis for the development and utilization of volatile oils from durian.

关 键 词：榴莲 挥发油 气相色谱-质谱联用法 

分 类 号：O656[理学—分析化学]