纳米Ni(OH)_2的制备及电化学性质测试的综合性实验设计  

Comprehensive Experimental Design Based on Synthesis and Electrochemical Properties of Nano-Ni(OH)_2

作　　者：王耀先[1] 赵晓军[1] 贺国旭[1] 王香[1] 

机构地区：[1]平顶山学院化学与环境工程学院,河南平顶山467000

出　　处：《实验科学与技术》2017年第4期31-33,53,共4页Experiment Science and Technology

基　　金：河南省教育厅科学技术研究重点项目(14B150050)

摘　　要：该文采用均相沉淀法制备了Ni(OH)_2纳米颗粒,运用X射线衍射技术和场发射扫描电镜对其结构和形貌进行表征,将其制作成电极,利用循环伏安和恒电流充放电技术对其电化学性质进行了研究。实践表明,因该实验涵盖的知识面广,有利于培养学生的科学素养和综合运用知识进行科学研究的能力,可以作为材料科学专业的综合性实验项目。Ni（OH） 2 nanoparticles were prepared by homogeneous precipitation method. The morphology and structure were characterized by X- ray diffraction（XRD） and field emission scanning electron microscopy （FESEM）respectively. Further investigation on the electrochemical performance of Ni （OH）2 nanoparticles which used as the electrode materials was studied by cyclic voltammetry and constant current charge and discharge technology. The designing experiment includes a lot of knowledge and it is beneficial to develop students scientific literacy and comprehensive use of knowledge to carry out scientific research. Thus it can be applied as a comprehen- sive experimental of project in materials science.

关 键 词：氢氧化镍 电化学性质 均相沉淀法 综合性实验 

分 类 号：O646[理学—物理化学]