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作 者:侯传信 LIU Guifang 党锋 ZHANG Zidong CHEN Ju
机构地区:[1]Key Laboratory for Liquid-Solid Structural Evolution & Processing of Materials Ministry of Education, Shandong University, Jinan 250061, China [2]Shandong Chunxu Chemical Design Co., Ltd., Jinan 250061, China
出 处:《Journal of Wuhan University of Technology(Materials Science)》2017年第4期871-874,共4页武汉理工大学学报(材料科学英文版)
基 金:Funded by the Qilu Program in Shandong University and the Natural Science Foundation of Shandong Province(ZR2014EMM001)
摘 要:Barium ferrite micro/nano fibers were successfully prepared via the electrostatic spinning by using dimethyl formamide(DMF) as the solvent, and poly vinyl pyrrolidone(PVP) as the spinning auxiliaries. Effects of strontium substitution on the structure, morphology, and magnetic properties were investigated by scanning electron microscope(SEM), X-ray diffraction analysis(XRD), and vibration sample magnetometer(VSM). XRD patterns of the samples confirm that pure barium ferrite fibers form, and the Sr substitution makes the main peaks(110),(107), and(114) move to right slightly. Also, the FE-SEM images show that the Sr substituted fibers can keep complete fibrous morphology. Moreover, the VSM results demonstrate that the saturation magnetization can reach 56.7 emu/g when the fibers are calcined at 800℃.Barium ferrite micro/nano fibers were successfully prepared via the electrostatic spinning by using dimethyl formamide(DMF) as the solvent, and poly vinyl pyrrolidone(PVP) as the spinning auxiliaries. Effects of strontium substitution on the structure, morphology, and magnetic properties were investigated by scanning electron microscope(SEM), X-ray diffraction analysis(XRD), and vibration sample magnetometer(VSM). XRD patterns of the samples confirm that pure barium ferrite fibers form, and the Sr substitution makes the main peaks(110),(107), and(114) move to right slightly. Also, the FE-SEM images show that the Sr substituted fibers can keep complete fibrous morphology. Moreover, the VSM results demonstrate that the saturation magnetization can reach 56.7 emu/g when the fibers are calcined at 800℃.
关 键 词:electrostatic spinning Sr substituted barium ferrite fibers magnetic properties
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