硫化钼/炭复合物的合成及其润滑性能的研究  

Synthesis and iubricant properties of molybdenum sulfide/carbon composites

作　　者：李江涛[1] 贾园[1] 沈萌 庄智 朱刚[1] 宋立美[1] 

机构地区：[1]陕西省表面工程与再制造重点实验室西安文理学院化学工程学院,陕西西安710065

出　　处：《化学工程师》2017年第9期1-3,17,共4页Chemical Engineer

基　　金：国家自然基金(No.21541009);西安市科技计划项目(No.CX1531WL13)

摘　　要：本文以钼酸铵与硫代乙酰胺分别为钼源和硫源,活性炭为碳源,采用溶剂热法制成二硫化钼/碳的复合物。采用粉末衍射、红外、扫描电镜、物理吸附等方法对不同条件下制备的产物进行组成和结构表征,检测产物的摩擦学性能,研究加热时间不同对产物的结构、成分和摩擦性能进行研究。MoS2/C composite were synthesized by solvothermal method using ammonium molybdate and thioac- etamide as molybdenum source and sulphur source. The composition and structure of products were characterized by XRD, vr-IR, SEM, and the influence of the synthesis conditions on products were investigated. The synthesis conditions （such as material structure, reaction time ） have significant effect on the morphology and friction prop- erties.

关 键 词：硫化钼 溶剂热反应 润滑性能 

分 类 号：TB332[一般工业技术—材料科学与工程]