2-(2,4-二氯苯基)-乙脒盐酸盐的合成与表征  

Synthesis and Characterization of 2-(2,4-dichlorophenyl) Acetamidine Hydrochloride

作　　者：张小春 李宗沅 吴正旭 Zhang Xiaochun, Li Zongyuan, Wu Zhengxu(Guangdong Open Laboratory of Chemical Engineering, Guangdong Petrochemical Research Institute, Guangzhou 510665, Chin)

机构地区：[1]广东省石油与精细化工研究院,广东广州510665

出　　处：《广东化工》2018年第5期1-2,共2页Guangdong Chemical Industry

基　　金：广州市科技计划项目:新型耐高温铜面防氧化剂关键材料合成与应用研究(项目编号:201707010499)

摘　　要：以2,4-二氯苯乙腈和氯化铵作原料,采用Pinner-碱催化法,合成了2-(2,4-二氯苯基)-乙脒盐酸盐,首次采用IR、核磁共振、质谱和离子色谱对结构进行了表征。2-（2,4-dichlorophenyl） acetamidine hydrochloride was synthesized by Pinner reaction between 2,4-dichlorobenzene acetonitrile and ammonium chloride catalyzed by alkali; for the first time, the structure of the target compound was comfirmed by FT-IR, 1HNMR, 13CNMR, MS, IC.

关 键 词：2 4-二氯苯乙腈 氯化铵 甲醇钠 Pinner法 

分 类 号：TQ[化学工程]