Alumina Ceramics Fabricated by in-situ Consolidation of Pre-gelling Starch  

作　　者：朱田丽 王友法 

机构地区：[1]State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology

出　　处：《Journal of Wuhan University of Technology(Materials Science)》2018年第3期758-766,共9页武汉理工大学学报（材料科学英文版）

基　　金：Funded by the National Key Research and Development Program of China(Nos.2017YFC1103800,2016YFC1101605);Wuhan Key Science and Technology Project(No.2017060201010191)

摘　　要：An in-situ consolidation method was developed and optimized to successfully fabricate alumina ceramics using pre-gelling starch. Our results showed that the obtained ceramics have more homogeneous microstructure, higher density, higher flexural strength, and favorable biocompatibility compared to the regular one. During the process, cornstarch granules swelled and deformed but no fracture was observed. After the cornstarch granules bursted, alumina particles were suspended uniformly in the three-dimensional network structure to generate a much smoother surface. Below 0.5 wt% higher cornstarch content increased the flexural strength of prepared ceramics, while above 0.5 wt% the mechanical properties were compromised. Therefore the cornstarch content of 0.5% was the optimal concentration to achieve the highest mechanical strength of the prepared ceramics, with a measured flexural strength of 341 MPa, and a relative density of 96.01%.An in-situ consolidation method was developed and optimized to successfully fabricate alumina ceramics using pre-gelling starch. Our results showed that the obtained ceramics have more homogeneous microstructure, higher density, higher flexural strength, and favorable biocompatibility compared to the regular one. During the process, cornstarch granules swelled and deformed but no fracture was observed. After the cornstarch granules bursted, alumina particles were suspended uniformly in the three-dimensional network structure to generate a much smoother surface. Below 0.5 wt% higher cornstarch content increased the flexural strength of prepared ceramics, while above 0.5 wt% the mechanical properties were compromised. Therefore the cornstarch content of 0.5% was the optimal concentration to achieve the highest mechanical strength of the prepared ceramics, with a measured flexural strength of 341 MPa, and a relative density of 96.01%.

关 键 词：pre-gelling starch in-situ consolidation alumina-ceramic flexural strength biocompatibility 

分 类 号：TQ174.758.11[化学工程—陶瓷工业]