锶钒杂多化合物的合成及性质  

Synthesis and properties of strontium-vanadium heteropoly compound

作　　者：邱磊 汤雨朦 李莲 邹水香 陈砚美 QIU Lei;TANG Yu-meng;LI Lian;ZOU Shui-xiang;CHEN Yan-mei(College of Chemistry and Chemical Engineering,Huanggang Normal University,Huanggang 438000,Hubei,China)

机构地区：[1]黄冈师范学院化学化工学院,湖北黄冈438000

出　　处：《黄冈师范学院学报》2018年第3期27-30,共4页Journal of Huanggang Normal University

基　　金：黄冈师范学院化学实验教学示范中心项目(zx201724;zj201722;zj201723)

摘　　要：本文合成了一新的锶钒杂多化合物[Sr3(V2O6)2(OH)2(H2O)6]n,并用X-射线单晶衍射对其结构进行了表征,结果表明该晶体为正交晶系,Cmc21空间群,其空间结构为三维网状。此外,还对此杂多化合物进行了一系列的表征,如:X-粉末衍射、元素分析,红外光谱和热稳定性分析等。A new heteropoly compound[Sr3（V2 O6）2（OH）2（H2 O）6]nhas been hydrothermally synthesized,its structure is characterized by X-ray single crystal diffractometer.The crystal structure determination reveals that compound displays3-D network structure,and crystallizes in the orthorhombic crystal system of the Cmc21 space group.And also it has been characterized by powder X-ray diffraction,elemental analysis,IR spectroscopy and thermal analysis.

关 键 词：杂多化合物 合成 性质 表征 

分 类 号：O626.21[理学—有机化学]