广谱高效防晒剂的制备及紫外屏蔽性能研究  

Preparation of Highly Effective Broad-Spectrum Sunscreen and the Studies of UV Shielding Property

作　　者：曾远娴 冯彩珠 陈凤桂 李光明 郑燕玲 刘菊兰 林典 刘燕[1] 林穗云[1] Zeng Yuanxian;Feng Caizhu;Chen Fenggui;Li Guangming;Zheng Yanling(School of Chemistry and Environment,Jiaying University,Meizhou 514015,China)

机构地区：[1]嘉应学院化学与环境学院,广东梅州514015

出　　处：《山东化工》2018年第16期1-2,5,共3页Shandong Chemical Industry

基　　金：广东省自然科学基金(2016A030307009);广东省大学生创新创业训练项目(201710582054);"攀登计划"广东大学生科技创新培育专项资金(201805)

摘　　要：以氯化锌和硬脂酸为原料,采用溶剂热法,一步制备硬脂酸修饰的ZnO纳米颗粒。用沉降实验、X-射线衍射仪(XRD)、红外光谱仪(IR)、扫描电镜(SEM)和紫外可见分光光度计等对样品进行表征。结果表明,样品属于红锌矿型合成纳米氧化锌,颗粒尺寸约为10~30 nm,在有机溶剂中具有良好的分散性好,在200 nm^400 nm的紫外线屏蔽率达到94.1%~98.9%,具有广谱高效的防晒效果。The stearic acid modified ZnO nanoparticles were successfully prepared by one-step solvothermal method and by using zinc chloride and stearic acid as raw material. The samples were characterized by sedimentation experiment,X-ray powder diffraction（ XRD）,infrared spectrometer（ IR）,scanning electron microscopy（ SEM） and ultraviolet and visible spectrophotometer. The results indicate that the sample is a synthetic nano Zn O of zincite,the nanoparticles with diameter in the range of 10 - 30 nm,and the SA-Zn O nanoparticles has excellent dispersion stability in organic solvent,its ultraviolet radiation screening factor is 94. 1% to 98. 9% at 200 - 400 nm,it has a broad spectrum and efficient sunscreen effect.

关 键 词：纳米氧化锌 制备 高效防晒剂 屏蔽率 

分 类 号：O647.2[理学—物理化学] TQ132.4[理学—化学]