用气相色谱法同时测定薄荷型卷烟滤嘴中的薄荷醇、三乙酸甘油酯和烟碱含量  

Simultaneous determination of the content of menthol,triacetin and nicotine in mint cigarette filter by gas chromatography

作　　者：许蔼飞[1] 章平泉[2] 范忠[1] 黄世杰[1] 陈志燕[1] 周芸[1] 唐桂芳[1] 朱静[1] 李小兰[1] 许春平[3] XU Aifei;ZHANG Pingquan;FAN Zhong;HUANG Shijie;CHEN Zhiyan;ZHOU Yun;TANG Guifang;ZHU Jing;LI Xiaolan;XU Chunpings(Technology Center,China Tobacco Guangxi Industrial Co.,Ltd.,Nanning 530001,China;Quality Management Department of Huaiyin Cigarette Factory,China Tobacco Jiangsu Industrial Co.,Ltd.,Huaian 223002,China;College of Food and Bioengineering,Zhengzhou University of Light Industry,Zhengzhou 450001,China)

机构地区：[1]广西中烟工业有限责任公司技术中心,广西南宁530001 [2]江苏中烟工业有限责任公司淮阴卷烟厂品质管理处,江苏淮安223002 [3]郑州轻工业学院食品与生物工程学院,河南郑州450001

出　　处：《轻工学报》2018年第5期53-59,共7页Journal of Light Industry

基　　金：国家自然科学基金联合基金项目(U1604176);广西中烟合作项目(201745000034020)

摘　　要：选择HP-Innowax毛细管色谱柱,以无水乙醇为萃取溶剂,采用气相色谱法同时测定薄荷型卷烟滤嘴中的薄荷醇、三乙酸甘油酯和烟碱含量.结果表明:薄荷醇、三乙酸甘油酯和烟碱分别在质量浓度0. 30～4. 80 g·L-1,0. 30～4. 80 g·L-1和0. 01～0. 16 g·L-1范围内线性关系良好,定量限分别为14. 4μg·支-1,29. 8μg·支-1和9. 6μg·支-1,3种目标物的加标回收率在97. 1%～103. 1%之间,使用该方法对7个薄荷型卷烟滤嘴样品进行测定,3种目标物的相对标准偏差均<3. 0%,爆珠薄荷型卷烟滤嘴中薄荷醇含量明显高于传统薄荷型卷烟滤嘴,而烟碱和三乙酸甘油酯含量变化无明显规律.HP-Innowax capillary column was selected and the content of menthol, triacetin and nicotine in mint cigarette filter was determined by gas chromatography with anhydrous ethanol as extraction solvent. The results showed that： The linear xelationship was good among menthol, triacetic acid and nicotine in the concentration range of 0.30 -4.80 g · L^-1 , 0.30 -4.80 g · L^-1 and 0.01 -0.16 g · L^-1 , respectively, the limit of quan- tification was 14.4 μg · branch^-1 ,29.8 μg · branch^-1 and 9.6 μg · branch^-1 , the spiked recoveries of the three targets ranged from 97.1% to 103.1% , and the detemnnation result of 7 mint cigarette filter samples by this method showed that the relative standard deviations （RSD） were less than 3.0%. The content of menthol in the menthol cigarette filter was significantly higher than that of the traditional menthol cigarette filter, while the change of nicotine and triacetin content had no obvious change.

关 键 词：气相色谱法 薄荷型卷烟滤嘴 薄荷醇 三乙酸甘油酯 烟碱 

分 类 号：TS411[农业科学—烟草工业]