3-氨基4-(叠氮乙酰胺基)呋咱合成  被引量：1

Synthesis of 3Amino4(azidoacetamido)Furazan</em> <p class='article-op'> <span id="bdshare" class="bdshare_t bds_tools get-codes-bdshare baidufx"><span><span class="bds_more" style="display: block; width: 62px; height: 29px; background: url(/images/share.gif) no-repeat!important; padding: 0;"></span></span></span> </p> <p class="article-source"> <a href ='/article/read.aspx?id=6819442' class='btnTitle btnIsView' target='_blank'><img alt='在线阅读' src='/images/btn-read.png'/></a><a class='btnTitle btnIsView' href="javascript:showdown('vdAq2IRi3oUkkIjHwbT8LYo7/voLZoeHW6z0pJ307RA=')"><img alt="下载全文" src="/images/btn-down.png" /></a> <input id="hiddowninfo" type="hidden" value="vdAq2IRi3oUkkIjHwbT8LYo7/voLZoeHW6z0pJ307RA="/> </p> <div class="collect" style="display: none"> <h5>我的收藏</h5> <div class="cnt"> <p> 名 称：<input type="text" name="collTitle" id="collSumTitle" /> </p> <p> 注 释：<input type="text" name="collRemark" id="collSumRemark" /> </p> <p style="text-align: center;"> <a href="javascript:void(0)" onclick="g_collectSumOk();"> <img width="65" height="17" src="/images_new/collect_ok.png" alt="完成" /></a> <a href="javascript:void(0)" onclick="g_collectSumCancel();"> <img width="65" height="17" src="/images_new/collect_no.png" alt="取消" /></a> </p> </div> </div> </div> <form name="wxTransfer" method="post"> <input type="hidden" name="lid" value="" /> <input type="hidden" name="sip" value="" /> <input type="hidden" name="date" value="" /> <input type="hidden" name="co" value="" /> <input type="hidden" name="Title_C" value="" /> <input type="hidden" name="Writers" value="" /> <input type="hidden" name="Name_C" value="" /> <input type="hidden" name="Num" value="" /> <input type="hidden" name="Years" value="" /> <input type="hidden" name="Volumn" value="" /> <input type="hidden" name="GCH" value="" /> <input type="hidden" name="Vol" value="" /> <input type="hidden" name="BookID" value="" /> <input type="hidden" name="SubjectNum" value="" /> <input type="hidden" name="SpecialNum" value="" /> <input type="hidden" name="mirrorName" value="" /> <input type="hidden" name="UserID" value="" /> <input type="hidden" name="UserName" value="" /> <input type="hidden" name="sourceID" value="" /> </form> <script type="text/javascript" src="/scripts/transfer.min.js"></script> <div class="article-detail"> <p class='author'><strong>作　　者：</strong><a href='/writer/article.aspx?id=100000008429893' target='_blank' ><b class='type_ico_id'></b></a><a href='/zk/search.aspx?key=A%3d%5b%e6%9d%8e%e6%88%98%e9%9b%84%5d' title='李战雄[1]'>李战雄[1]</a> <a href='/writer/article.aspx?id=100000008203386' target='_blank' ><b class='type_ico_id'></b></a><a href='/zk/search.aspx?key=A%3d%5b%e5%94%90%e6%9d%be%e9%9d%92%5d' title='唐松青[1]'>唐松青[1]</a> <a href='/writer/article.aspx?id=100000029712302' target='_blank' ><b class='type_ico_id'></b></a><a href='/zk/search.aspx?key=A%3d%5b%e5%88%98%e9%87%91%e6%b6%9b%5d' title='刘金涛[1]'>刘金涛[1]</a> <a href='/writer/article.aspx?id=100000013587650' target='_blank' ><b class='type_ico_id'></b></a><a href='/zk/search.aspx?key=A%3d%5b%e9%92%b1%e5%9b%bd%e5%85%b4%5d' title='钱国兴[1]'>钱国兴[1]</a> <em> </em></p><p class='organ'><strong>机构地区：</strong><a href='/organ/article.aspx?id=18940&subid=&showname=&searchtype=' target='_blank'><b class='type_ico_id'></b></a><a href='/zk/search.aspx?key=S%3d%e4%b8%ad%e5%9b%bd%e7%a7%91%e5%ad%a6%e9%99%a2%e4%b8%8a%e6%b5%b7%e6%9c%89%e6%9c%ba%e5%8c%96%e5%ad%a6%e7%a0%94%e7%a9%b6%e6%89%80' title='[1]中国科学院上海有机化学研究所,上海200032'>[1]中国科学院上海有机化学研究所,上海200032</a> <em> </em></p><p class='from'><strong>出　　处：</strong><a href='/journal/summary.aspx?gch=90247X' target='_blank'><b class='type_ico_id'></b></a><a href='/zk/search.aspx?key=J%3d%5b%e5%90%ab%e8%83%bd%e6%9d%90%e6%96%99%5d' title='含能材料'>《含能材料》</a>2002年第3期112-113,共2页<em>Chinese Journal of Energetic Materials</em></p><p class='fund'><strong>基　　金：</strong>.NULL.</p><p class='abstrack'><strong>摘　　要：</strong>以3,4 二氨基呋咱(DAF)分别和氯乙酰氯、溴乙酰溴缩合得到了单取代乙酰化产物,进一步叠氮化得到的3 氨基 4 (叠氮乙酰胺基)呋咱为高氮含量的呋咱含能衍生物。<em><Abstrcat> The acetylation of 3,4diaminofurazan (DAF) was studied in this paper. By the reaction of DAF with chloroacetyl chloride and bromoacetyl bromide respectively, the substituted acetyl furazano derivatives were obtained. Then 3amino4(azidoacetamido)furazan was obtained as an high nitrogen content furazano energetic derivative by treating these two intermediates with sodium azide. </em></p><p class='subject'><strong>关 键 词：</strong><a href='/zk/search.aspx?key=K%3d%5b3%5d' title='3'>3</a> <a href='/zk/search.aspx?key=K%3d%5b4%e4%ba%8c%e6%b0%a8%e5%9f%ba%e5%91%8b%e5%92%b1%5d' title='4二氨基呋咱'>4二氨基呋咱</a> <a href='/zk/search.aspx?key=K%3d%5b%e5%8f%a0%e6%b0%ae%e4%b9%99%e9%85%b0%e8%83%ba%e5%9f%ba%5d' title='叠氮乙酰胺基'>叠氮乙酰胺基</a> <a href='/subject/article.aspx?id=8332891' target='_blank'><b class='type_ico_id'></b></a><a href='/zk/search.aspx?key=K%3d%5bDAF%5d' title='DAF'>DAF</a> <a href='/subject/article.aspx?id=976023' target='_blank'><b class='type_ico_id'></b></a><a href='/zk/search.aspx?key=K%3d%5b%e4%b9%99%e9%85%b0%e5%8c%96%5d' title='乙酰化'>乙酰化</a> <a href='/zk/search.aspx?key=K%3d%5b%e5%8f%a0%e6%b0%ae%e5%8c%96%5d' title='叠氮化'>叠氮化</a> <a href='/subject/article.aspx?id=1355105' target='_blank'><b class='type_ico_id'></b></a><a href='/zk/search.aspx?key=K%3d%5b%e7%82%b8%e8%8d%af%5d' title='炸药'>炸药</a> </p><p class='class'><strong>分 类 号：</strong><a href='/zk/search.aspx?key=C%3dTQ56' title='TQ56'>TQ56</a>[<a href = '/domain/article.aspx?id=132' >化学工程—炸药化工</a>] <a href='/zk/search.aspx?key=C%3dO626' title='O626'>O626</a>[<a href = '/domain/article.aspx?id=408' >理学—有机化学</a>] </p> </div> <div id="content_wzxg" name="wzxg" class="article-graph"> <object width="695" height="250" classid="clsid:D27CDB6E-AE6D-11cf-96B8-444553540000" id="FlashID"> <param value="../flash/relation.swf" name="movie"> <param value="high" name="quality"> <param value="opaque" name="wmode"> <param value="6.0.65.0" name="swfversion"> <param value="dataUrl=/ajax/articlerelativegraph.ashx?id=6819442" name="flashVars"> <embed width="695" height="250" src="../flash/relation.swf" type="application/x-shockwave-flash" quality="high" wmode="opaque" flashvars="dataUrl=/ajax/articlerelativegraph.ashx?id=6819442"> </embed> 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