新型助交联剂TMAIC的合成  

Synthesis of New Aid Crosslinking Agent TMAIC

作　　者：季成官[1] JI Chengguan(Shanxi Chemical Research Institute Co. Ltd., Taiyuan 030001, China)

机构地区：[1]山西省化工研究所(有限公司),山西太原030001

出　　处：《化工技术与开发》2016年第12期8-10,共3页Technology & Development of Chemical Industry

摘　　要：本文介绍了TMAIC的合成方法,研究了各种工艺参数对合成反应的影响。得出最佳工艺条件为:甲基氯丙烯与氰酸钠的摩尔比为1.05,滴加温度以110℃为宜,反应温度应该控制在130℃左右,搅拌下反应3h,产品收率达84%。The synthesis of TMAIC was introduced, the effect of different technic parameters in the synthesis were studied. The best technology parameters were obtained:the molar ratio of methyl allyl chloride to sodium cyanate was 1.05, droped at 110℃, the reaction temperature was about 130℃, and stirred for 3h. Under the optimum conditions, the yield was about 84 %.

关 键 词：甲基三烯丙基异氰脲酸酯 交联剂 氰酸钠 

分 类 号：TQ314.24[化学工程—高聚物工业]