飞行时间质谱技术在水果、蔬菜与茶叶中农药残留分析中的应用  

Applications of Time of Flight Mass Spectrometry in Analysis on Pesticide Residues in Fruits,Vegetables and Tea

作　　者：绳慧珊 张新忠[1,3] 王新茹 钟青 罗逢健 崔新仪[2] 周利 孙荷芝 杨梅[1] 楼正云 陈宗懋 SHENG Hui-shan;ZHANG Xin-zhong;WANG Xin-ru;ZHONG Qing;LUO Feng-jian;CUI Xin-yi;ZHOU Li;SUN He-zhi;YANG Mei;LOU Zheng-yun;CHEN Zong-mao(Research Center of Quality Safety for Agricultural Products,Tea Research Institute,Chinese Academy of Agricultural Sciences,Hangzhou 310008,China;Collage of Horticulture and Landscape,Tianjin Agricultural University,Tianjin 300384,China;Key Laboratory of Tea Quality and Safety Control,Ministry of Agriculture,Hangzhou 310008,China)

机构地区：[1]中国农业科学院茶叶研究所农产品质量安全研究中心,浙江杭州310008 [2]天津农学院园艺园林学院,天津300384 [3]农业部茶叶质量安全控制重点实验室,浙江杭州310008

出　　处：《分析测试学报》2018年第2期139-153,共15页Journal of Instrumental Analysis

基　　金：国家自然科学基金资助面上项目(31772077);中央级科研院所基本科研业务费专项资助(1610212017014);国家茶叶产业技术体系(CARS-23);中国农业科学院创新工程

摘　　要：飞行时间质谱(TOF-MS)是一种速度快、范围广、灵敏度高、分辨率高的质谱技术,相对于常规离子阱、四极杆质谱仪,具有定性能力更强、通量筛查能力更高的优点,TOF-MS技术的不断改进,为科研工作者提供了更好的研究手段,其在农产品质量安全农药残留定性定量筛查分析中也日益受到青睐。该文针对2010年来国内外期刊上发表的TOF-MS技术在水果、蔬菜和茶叶中农药残留分析上的应用文献,从TOF-MS与气相色谱、液相色谱和合相色谱联用3个方面上的应用出发,进行综述分析,并对该技术在水果、蔬菜和茶叶农药残留分析上的发展前景进行了展望。Time-of-flight mass spectrometry(TOF-MS)is a kind of mass spectrometric technique with high scan speed,wide scan range,high sensitivity and high mass resolution abilities.Compared with the conventional ion trap and quadruple mass spectrometry,TOF-MS has higher qualitative and throughput screening abilities.The applications of qualitation and quantitation on pesticide residues in the field of quality and safety on agricultural products have become more and more important.With the continued improvement and development of TOF-MS technique,it has been considered a powerful research tool for researchers.In this paper,the literatures on TOF-MS applications in analysis of pesticide residues in fruit,vegetable and tea,published at home and abroad since 2010,are reviewed in three aspects where it is coupled with gas chromatography,liquid chromatography and convergence chromatography.The development prospect of this TOF-MS technique in pesticide residue analysis of fruits,vegetables and tea is also prospected.

关 键 词：飞行时间质谱 水果 蔬菜 茶叶 农药残留分析 综述 

分 类 号：O657.63[理学—分析化学]