3,5-二叔丁基水杨醛肟的制备方法  

Synthesis of 3,5-di-tert-butyl Salicylaldoxime

作　　者：牛学丽 邢菲菲[1] 杨华 NIU Xue-li;XING Fei-fei(Shandong Provincial Key Laboratory of Chemical Energy Storage and Novel CellTechnology, Liaocheng University,Shandong Liaocheng 252059,China;Jincheng Institute of technology,Shanxi Jincheng 048026,China)

机构地区：[1]聊城大学山东省化学储能与新型电池技术重点实验室,山东聊城252059 [2]晋城职业技术学院,山西晋城048026

出　　处：《太原科技大学学报》2018年第6期478-481,共4页Journal of Taiyuan University of Science and Technology

基　　金：国家自然科学青年基金(21701078)

摘　　要：为了研究3,5-二叔丁基水杨醛肟的制备方法,并提高其产率,试验了不同反应条件下制备3,5-二叔丁基水杨醛肟的产率。最终通过正交实验确定了制备3,5-二叔丁基水杨醛肟的最佳条件。最佳反应条件为:室温反应10 h,调p H值为4,产率可达94. 8%.本制备方法与已报道的类似合成方法比较,在保证产率的前提下,提高了原料使用和制备过程的安全性。In order to study the preparation method of 3,5-di-tert-butyl salicylaldoxime and improve its yield,the different reaction conditions have been studied.The optimum conditions for the preparation of 3,5-di-tert-butyl salicylaldoxime were determined by orthogonal experiment.The optimum reaction conditions were as follows:room temperature reaction for 10 hours,adjusting pH value to 4,and the yield is over 94.8%.Compared with the similar synthesis method reported in this paper,the safety of the raw materials and the preparation process is improved on the premise of ensuring the yield.

关 键 词：3 5-二叔丁基水杨醛肟 制备 最佳反应条件 

分 类 号：O622.6[理学—有机化学]