电感耦合等离子体原子发射光谱(ICP-AES)法测定H-ZF类光学玻璃中锑含量  

Determination of Stibium in H-ZF Types Optical Glasses by ICP-AES

作　　者：杨斌 胡向平 何蓉 邬理凡 王德国 YANG Bin;HU Xiangping;HE Rong;WU Lifan;WANG Deguo(Hubei New Huaguang Information Materials Co.,Ltd.,Xiangyang,Hubei 441057,China)

机构地区：[1]湖北新华光信息材料有限公司,湖北襄阳441057

出　　处：《中国无机分析化学》2018年第6期21-24,共4页Chinese Journal of Inorganic Analytical Chemistry

摘　　要：采用ICP-AES检测H-ZF类玻璃中锑含量,对共存元素产生的光谱干扰进行校正,并运用离峰扣除背景消除玻璃基体钛铌的干扰。建立简单可靠的分析方法,加标回收率为95%～110%,相对标准偏差≤2%,适合日常的快速分析需要。An ICP-AES method for the determination of Sb element in H-ZF types optical glass was proposed.The spectral interferences of co-existing elements were corrected and used off-peak subtraction of background to eliminate the interference of glass matrix titanium niobium.The recovery rate was 95%-110%,the relative standard deviation was less than 2%.The proposed analysis method is simple and reliable,can meet the requirement of daily rapid analysis.

关 键 词：光学玻璃 锑 ICP-AES 

分 类 号：O657.31[理学—分析化学] TH744.11[理学—化学]