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作 者:白妮 刘杰[2] 张红梅 杨振萍 Bai Ni;Liu Jie;Zhang Hongmei;Yang Zhenping(Yan ′an Municipal Hospital of Traditional Chinese Medicine,Yan ′an 716000,China;Yan ′an Disease Prevention and Control Center,Yan ′an 716000,China)
机构地区:[1]延安市中医医院,延安716000 [2]延安市疾病预防控制中心,延安716000
出 处:《世界中医药》2019年第2期301-305,共5页World Chinese Medicine
基 金:国家自然科学基金青年基金项目(81601081)
摘 要:目的:建立清热解毒口服液的质量控制方法。方法:选取薄层色谱法,鉴别连翘、黄柏、栀子、赤芍等主要药效成分;采用高效液相色谱法测定方中君药金银花的主要药效成分绿原酸的含量。结果:确立了清热解毒口服液中连翘、黄柏、栀子、赤芍的薄层色谱鉴别方法。在选定的高效液相色谱条件下,建立了清热解毒口服液中绿原酸的含量测定方法,其方法学均符合药典要求。结论:本实验建立的定性鉴别和含量测定方法简便、准确、重复性好,适用于清热解毒口服液的质量控制。Objective:To improve the quality standard of Qingre Jiedu Oral Solution.Methods:TLC(Thin-Layer Chromatography)methods were used for the qualitative identification of Forsythiae Fructus,Cortex Phellodendri,Fructus Gardeniae and Radix Paeoniae Rubra,and HPLC(High Performance Liquid Chromatography)method was used to determine chlorogenic acids of the main drug Flos Lonicerae.Results:Identification method of the TLC about Forsythiae Fructus,Cortex Phellodendri,Fructus Gardeniae and Radix Paeoniae Rubra etc in Oral Solution was established.Under the selected conditions of HPLC,an identification method for chlorogenic acids in Oral Solution was established and the methodology complies with the requirements of Chinese Pharmacopeia.Conclusion:The identification and quantitative determination method is simple,accurate and reproducible,which can be applied to the quality control of Qingre Jiedu Oral Solution.
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