4-氨基苯基-β-羟乙基砜硫酸酯重氮化反应的研究  

Study on Diazotization of 4-Aminophenyl-beta-hydroxyethyl Sulfone Sulfate

作　　者：曹世川 张克栋 CAO Shi-chuan;ZHANG Ke-dong

机构地区：[1]不详

出　　处：《染料与染色》2019年第3期25-26,42,共3页Dyestuffs and Coloration

摘　　要：本文详细研究了4-氨基苯基-β-羟乙基砜硫酸酯的重氮化条件,得出反应的最佳条件为:反应温度10~15℃,对位酯与酸摩尔比1∶1.1,反应液浓度15%,重氮化时间1 h。此条件重氮化可以有效降低原料成本、减少人工劳动同时减少污染,在染料生产上具有重要的指导意义。The diazotization conditions of 4-aminophenyl-beta-hydroxyethyl sulfone sulfate were studied in detail in this paper.The optimum reaction conditions were obtained as follows:temperature 10~15 ℃,acid molar ratio 1∶1.1,concentration 15%,diazotization time 1 hour.Diazotization under this condition could effectively reduce the cost of raw materials,labor and pollution.It has an important guiding significance in dye production.

关 键 词：4-氨基苯基-β-羟乙基砜硫酸酯 对位酯 重氮化 

分 类 号：TQ612.2[化学工程—精细化工]