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作 者:Pengfei Xie Wenyuan Ji Zhigang Wei
机构地区:[1]School of Materials Science and Engineering, Shenzhen Engineering University, Guangdong, China
出 处:《Characterization and Application of Nanomaterials》2018年第1期40-48,共9页纳米科学的表征与应用
摘 要:With the progress of science and technology, the research and development of silver nanoparticles has also developed. This paper attempts to prepare a silver nanoparticle by electrolyzing AgNO3 solution with electrochemical reduction method and citric acid as a complexing agent in a certain current and time. The crystal morphology and sample purity of silver nanoparticles were analyzed by X-ray diff ractometer. The crystal structure of the nanoparticles was analyzed by scanning electron microscopy (SEM). The crystal structure of the nanoparticles was analyzed by X-ray diff raction. The particle size distribution of the particles was in the range of 125-199 nm, and the carbon paste electrode was modifi ed with the prepared silver nanoparticles. The electrocatalytic activity of the carbon paste electrode was preliminarily explored.
关 键 词:SILVER NANOPARTICLES ELECTROLYSIS PREPARATION CHARACTERIZATION
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