3-氯-2-氟苯磺酰胺的确认和表征  

Identification and Characterization of 3-Chloro-2-fluorobenzene Sulfonamide

作　　者：周永生[1] 方建波[1] 朱洪武 顾浩[1] Zhou Yongsheng;Fang Jianbo;Zhu Hongwu;Gu Hao(School of Petrochemical Engineering,Changzhou University,Changzhou,Jiangsu 213164,China;Nanjing Langquan Science and Technology Industrial Company Limited,Nanjing,Jiangsu 210014,China)

机构地区：[1]常州大学石油化工学院,江苏常州213164 [2]南京朗全科技实业有限公司,江苏南京210014

出　　处：《化学世界》2019年第10期701-705,共5页Chemical World

摘　　要：试制了3-氯-2-氟苯磺酰胺(CFBS)样品,用1 H NMR、13C-NMR、ESI-MS、HPLC对其分子结构、分子量和质量分数进行了确认,对该样品进行IR、XRD和熔点表征。结果表明,该样品确认为CFBS,质量分数≥99.8%,熔点范围为156.2~157.3℃。3-Chloro-2-fluorobenzene sulfonamide(CFBS)was prepared and its molecular structure,molecular weight and mass fraction were confirmed by 1 H NMR,13 C NMR,ESI-MS and HPLC.In addition,the compound was characterized by IR,XRD and melting point instrument.The results show that the mass fraction is above 99.8%,its melting point is 156.2~157.3℃.

关 键 词：3-氯-2-氟苯磺酰胺 确认 表征 熔点 熔程 

分 类 号：O621.256.4[理学—有机化学]