Examination of Polymeric Azomethine Compounds and Their Transition Metal Complexes by Using XRF and XRD Technique  

作　　者：Omer Sogut Betül Demirezen Kara Gokhan Apaydin Erhan Cengiz Ayse Kazanc 

机构地区：[1]Kahramanmaras Sutcu Imam University,Faculty of Science and Letters,Department of Physics,Kahramanmaras,Turkey [2]Karadeniz Technical University,Faculty of Science,Department of Physics,Trabzon,Turkey [3]Alanya Alaaddin Keykubat University,Faculty of Engineering,Engineering Basic Sciences Department,Antalya,Turkey [4]Kahramanmaras Sutcu Imam University,Faculty of Science and Letters,Department of Chemistry,46100 Kahramanmaras,Turkey

出　　处：《光谱学与光谱分析》2020年第1期328-332,共5页Spectroscopy and Spectral Analysis

基　　金：Scientific Research Fund of Kahramanmaras Sutcu Imam University,Turkey(2012/3-7YLS)

摘　　要：In this study,the electronic transition properties and structural analysis of the metal complexes(Ni(Ⅱ),Co(Ⅱ),Cu(Ⅱ)and Mn(Ⅱ))of three different polymer ligands were performed by using XRF and X-ray diffraction(XRD)techniques,respectively.The structural analysis of the polymers and their complexes were performed by XRD technique and some of the polymers were found to be in the face-centred cubic(fcc)structure.In addition,the values of the present K X-ray intensity ratios are significantly greater than the values reported in literature.In this study, the electronic transition properties and structural analysis of the metal complexes(Ni(Ⅱ), Co(Ⅱ), Cu(Ⅱ) and Mn(Ⅱ)) of three different polymer ligands were performed by using XRF and X-ray diffraction(XRD) techniques, respectively. The structural analysis of the polymers and their complexes were performed by XRD technique and some of the polymers were found to be in the face-centred cubic(fcc) structure. In addition, the values of the present K X-ray intensity ratios are significantly greater than the values reported in literature.

关 键 词：XRF XRD Polymeric azomethine compounds and transition metal complexes 

分 类 号：O657.3[理学—分析化学]