毛细管气相色谱法分析间苯二甲胺  

Analysis of m-Phenylene Dimethylamine by Gas Chromatography

作　　者：王燕[1,2] 臧阳陵 罗先福[1,2] 李萍 刘国文[1,2] 周勇 WANG Yan;ZANG Yang-ling;LUO Xian-fu;LI Ping;LIU Guo-wen;ZHOU Yong(National Engineering Research Center for Agrochemicals,Hunan Research Institute of Chemical Industry,Changsha 410007,China;Hunan Province Key Laboratory for Agrochemicals,Changsha 410014,China)

机构地区：[1]湖南化工研究院国家农药创制工程技术研究中心,湖南长沙410014 [2]农用化学品湖南省重点实验室,湖南长沙410014

出　　处：《精细化工中间体》2019年第5期66-67,72,共3页Fine Chemical Intermediates

基　　金：湖湘青年英才项目资助（2019RS2060）

摘　　要：采用气相色谱法,以正十四烷为内标物,EC-1毛细管柱分离和氢火焰离子化检测器,对间苯二甲胺反应液进行定量分析。结果表明:方法的标准偏差为0.20,变异系数为3.0%,回收率为99.06%~101.42%;线性相关系数为0.9995。Gas chromatography was used to isolate n-tetradecane with EC-1 capillary column and hydrogen flame ionization detector. m-Phenylene dimethylamine was quantitatively analyzed.The results show that the standard deviation of the method is 0.20, the coefficient of variation was 3.0%, the recovery rate was 99.06% ~101.42%, the linear correlation coefficient was 0.999 5.

关 键 词：间苯二甲胺 毛细管气相色谱 分析 

分 类 号：O6576.7[理学—分析化学]