对氨基苯酚的合成工艺优化  

Optimization of Synthetic Process of P-aminophenol

作　　者：毛东东 王思雨 张磊 Mao Dongdong;Wang Siyu;Zhang Lei(Medical College,Pingdingshan University,Pingdingshan 467000,China)

机构地区：[1]平顶山学院医学院,河南平顶山467000

出　　处：《广东化工》2020年第16期15-16,40,共3页Guangdong Chemical Industry

摘　　要：本文以亚硝酸钠、苯酚为原料先制得对亚硝基苯酚,再用硫化钠还原制得对氨基苯酚。对还原反应采用正交试验进行工艺研究。优化后的工艺反应条件稳定,收率较原来提高了3.5%,具有一定的应用价值,为对氨基苯酚的工业化生产提供了依据。In this paper, p-nitrophenol was prepared from sodium nitrite and phenol, and then p-aminophenol was prepared by reduction of sodium sulfide. The reduction reaction was studied by orthogonal test. The optimized reaction conditions were stable and the yield was 3.5 % higher than the original one, which had certain application value and provided a basis for the industrial production of p-aminophenol.

关 键 词：对氨基苯酚 工艺优化 正交实验法 

分 类 号：TQ[化学工程]