石墨烯材料表面含氧官能团的表征研究  

Analysis of oxygen-containing functional groups on the surface of graphene material

作　　者：白云 李琴梅[1] 刘奕忍[1] 胡光辉[1] 陈成猛[2] 黄显虹[2] 陈新启 王大海 张梅[1] 刘伟丽[1] Bai Yun;Li Qinmei;Liu Yiren;Hu Guanghui;Chen Chengmeng;Huang Xianhong;Chen Xinqi;Wang Dahai;Zhang Mei;Liu Weili(Beijing Key Laboratory of Organic Materials Testing Technology and Quality Evaluation,Key Laboratory of Analysis and Testing,Beijing Academy of Science and Technology,Beijing Centre for Physical and Chemical Analysis,Beijing 100094,China;Institute of Coal Chemistry,Chinese Academy of Sciences,Taiyuan 030001,China)

机构地区：[1]有机材料检测技术与质量评价北京市重点实验室,北京市食品安全分析测试工程技术研究中心,北京市理化分析测试中心,北京100094 [2]中国科学院山西煤炭化学研究所,太原030001

出　　处：《分析仪器》2020年第4期83-88,共6页Analytical Instrumentation

基　　金：国家重点研发计划“石墨烯等碳基纳米材料NQI技术研究、集成与应用”之课题“石墨烯等碳基纳米材料标准研制及应用”(2016YFF0204302);北京市科学技术研究院2018年度青年骨干计划(YC201819);北京市科学技术研究院萌芽计划“药用滑石粉中金属元素的X射线荧光光谱测定方法开发”(GS201808)。

摘　　要：石墨烯是一种具有二维结构的新型碳纳米材料,特有的物理结构赋予其诸多优异性能。对石墨烯材料表面含氧官能团的类别和定性定量分析方法如傅里叶变换红外光谱法(FTIR)、X射线光电子能谱(XPS)和Boehm滴定法等进行了综述,结合3种表征技术分析了石墨烯材料表面含氧官能团的种类和含量。The types of functional groups and different methods for determination of these groups on graphene material were reviewed.The characterization methods such as Fourier transform-infrared spectrometer(FTIR),X-ray photoelectron spectroscopy(XPS)as well as Boehm titration were briefly described and their relative problems that may arise were discussed in detail.

关 键 词：石墨烯 官能团 类别 表征 

分 类 号：TQ127.11[化学工程—无机化工] TB383.1[一般工业技术—材料科学与工程]