几种N-亚胺喹唑啉叶立德化合物的制备与表征  

Synthesis and Characterization of N-Iminoquinazolinium Ylide Compounds

作　　者：徐瑛 罗金辉 冯海燕 王涛[2] 罗劲[3] XU Ying;LUO Jin-hui;FENG Hai-yan;WANG Tao;LUO Jin(Department of Ecology and Environment of Xinyu City,Xinyu 338000,China;College of Chemistry and Chemical Engineering,Jiangxi Normal University,Nanchang 330022,China;Analytical&Testing Center,Jiangxi Normal University,Nanchang 330022,China)

机构地区：[1]新余市生态环境局,江西新余338000 [2]江西省化学生物学重点实验室,江西师范大学化学化工学院,江西南昌330022 [3]江西师范大学分析测试中心,江西南昌330022

出　　处：《精细化工中间体》2020年第4期54-56,72,共4页Fine Chemical Intermediates

基　　金：江西省教育厅科学技术青年基金(GJJ150326)。

摘　　要：以取代邻硝基苯甲醛为初始原料,经3步反应合成了6个新型的N-亚胺喹唑啉叶立德化合物(1a^1f),产物经核磁共振氢谱、碳谱、红外光谱和高分辨质谱确证。Six new N-iminoquinazolinium ylide compounds(1a^1f)were synthesized in three steps using substituted o-nitrobenzaldehyde as the starting material.The structures of the target compounds were elucidated by 1H NMR,13C NMR,FT-IR and HR-MS.

关 键 词：邻硝基苯甲醛 合成 N-亚胺喹唑啉叶立德 

分 类 号：O626.4[理学—有机化学]