微乳液基法制备超细钒锆蓝色料的研究  

Investigation on the Ultrafine V-ZrSiO4 Pigment Prepared by Microemulsion-based Method

作　　者：马岚[1] 吴滨 鲍志蕾 汪其堃 MA Lan;Wu Bin;BAO Zhilei;WANG Qikun(School of Material Science and Engineering,Jiangxi Ceramic and Art Institute,Jingdezhen 333001,China;Jingdezhen KITO Ceramics Co.,Ltd,Jingdezhen 333400,China;School of Materials Science and Engineering,Jingdezhen Ceramic Institute,Jingdezhen 333403,China)

机构地区：[1]江西陶瓷工艺美术职业技术学院材料与机械工程学院,景德镇333001 [2]景德镇金意陶陶瓷有限公司,景德镇333400 [3]景德镇陶瓷大学材料科学与工程学院,江西景德镇333403

出　　处：《中国陶瓷》2020年第11期64-70,共7页China Ceramics

基　　金：江西省教育厅科技项目(GJJ191297)。

摘　　要：通过微乳液基法制备获得了两种形貌各异的超细钒锆蓝色料,并对两种色料的性能进行了对比研究。实验结果表明,溶胶凝胶微乳液法(SGM)能够得到中位径(D50)为2.114μm的球形色料;而溶胶凝胶微乳液水热法(SGMH)能够得到中位径(D50)为0.754μm的柱状色料。两种钒锆蓝色料在透明釉中均表现出良好的热稳定性及化学稳定性,其中超细柱状色料呈现出优异的着色性能,这为陶瓷喷墨打印技术提供了新的选择。In this paper,ultrafine V-ZrSiO4 pigment with two kinds of morphologies were prepared by microemulsion-based methods,and the performance of two pigment were investigated.The experimental results show that a spherical pigment with a median diameter(D50)of 2.114μm can be obtained by solgel-microemulsion method(SGM);and a columnar V-ZrSiO4 pigment with a median diameter(D50)of 0.754μm can be obtained by sol-gel microemulsion-hydrothermal method(SGMH).The two kinds of pigments both show good thermal and chemical stability in the transparent glaze.Moreover,the ultra-fine columnar pigment shows excellent coloring performance,which provides a new choice for ceramic inkjet printing technology.

关 键 词：色料 超细 钒锆蓝 微乳液 

分 类 号：TQ174.43[化学工程—陶瓷工业]