抗氧剂565的合成  

Synthesis of Antioxidant 565

作　　者：高俊峰 李河川 王跃 Gao Junfeng;Li Hechuan;Wang Yue(Baoding Lucky Chemical Company Limited,Baoding,Hebei 071054,China)

机构地区：[1]保定市乐凯化学有限公司,河北保定071000

出　　处：《信息记录材料》2020年第12期1-2,共2页Information Recording Materials

摘　　要：本文通过合成的6-(4-羟基-3,5-二叔丁基苯氨基)-2,4-二氯-1,3,5-三嗪与正辛硫醇反应,得到抗氧化剂565。考察了物料配比、反应时间、析出溶剂等对反应的影响,确定了最佳反应条件,产品收率稳定在92%左右。Antioxidant 565 was synthesized by the reaction of 6-(4-hydroxy-3,5-di-tert-butylphenylamino)-2,4-dichloro-1,3,5-triazine with n-octyl mercaptan.The effects of material ratio,reaction time and precipitation solvents on the reaction were investigated.The optimum reaction conditions were determined.The yield of the product was stable at about 92%.

关 键 词：6-(4-羟基-3 5-二叔丁基苯氨基)-2 4-二氯-1 3 5-三嗪 正辛硫醇 抗氧剂565 

分 类 号：TQ243.1[化学工程—有机化工]