基于GC-MS法检测纺织品中17种有机锡化合物  

Determination of seventeen organotin compounds in textile by GC-MS

作　　者：陈璐[1] 吴东晓[1] 曹石淼 谭玉静[1] CHEN Lu;WU Dongxiao;CAO Shimiao;TAN Yujing(Shanghai Institue of Quality Inspection and Technical Research,Shanghai 200040,China)

机构地区：[1]上海市质量监督检验技术研究院,上海200040

出　　处：《纺织检测与标准》2020年第6期9-13,共5页Textile Testing and Standard

摘　　要：使用外标法,建立一种使用气质(GC-MS)联用仪检测纺织品中潜在的17种有机锡化合物的方法,并确定优化的衍生化前处理条件,即:pH值4.0,衍生化时间30 min,衍生试剂用量1.00 mL。在此方法条件下可以方便、快速地检测出17种有机锡化合物。希望研究结果可为相关研究和检测提供帮助。The determination of seventeen organotin compounds in textile by GC-MS was established by using external stangard in the article.The pre-processing condition was determined as pH 4.0,time of derivative 30 min,dosage of derivative reagent 1.00 mL.Seventeen organotin compounds could be conveniently and rapidly detected in the condition of the method.The research result was hoped to afford the help for related research and detection.

关 键 词：外标法 气质联用仪 有机锡化合物 衍生化 

分 类 号：TS107[轻工技术与工程—纺织工程]