紫外线吸收剂UV-531合成工艺研究  

Synthesis Process of the Ultraviolet Light Absorber UV-531

作　　者：鲍芃丞 毕莹 田军 宋歌 张会京 范小鹏 孙春光 Bao Pengcheng;Bi Ying;Tian Jun;Song ge;Zhang Huijing;Fan Xiaopeng;Sun Chunguang(Rianlon Corporation,Tianjin,300450,China)

机构地区：[1]天津利安隆新材料股份有限公司,天津300384

出　　处：《塑料助剂》2020年第6期17-19,共3页Plastics Additives

摘　　要：在传统UV-531合成方法的基础上,对UV-531合成工艺进行进一步研究,采用KI与PEG-400作为催化剂,极大提高反应速率,减少副产物生成,在此反应条件下,采用过滤去除盐等固体杂质,方便工业操作,最终UV-531收率可以达到95.8%,HPLC纯度99.7%。Based on the traditional synthetic methods of UV-531,such synthetic process was further studied with both KI and PEG-400 as the catalyst so as to improve the reaction rate and reduce the by-products generated.Under the above-mentioned reaction conditions,filter was used to remove salt and other solid impurities,as a result,the UV-531 yield rate reached up to 95.8%with the HPLC purity of 99.7%.

关 键 词：紫外线吸收剂UV-531 合成 PEG-400 催化剂 

分 类 号：TQ320.4[化学工程—合成树脂塑料工业]