多溴联苯醚的GC-MS/MS分析方法探讨  

Analysis of polybrominated diphenyl ethers by GC-MS/MS

作　　者：陈璐 陈影 Chen Lu;Chen Ying(Jiangsu Society For Environmental Sciences,Nanjing,Jiangsu 210036,China;Jiangsu SinoUnison,Technology Co.,Ltd.,Nanjing,Jiangsu 210061,China)

机构地区：[1]江苏省环境科学学会,江苏南京210061 [2]江苏中谱检测有限公司,江苏南京210061

出　　处：《污染防治技术》2020年第6期39-41,共3页Pollution Control Technology

摘　　要：本文将建立多溴联苯醚(PBDEs)的气相色谱串联质谱(GC-MS-MS)仪器分析方法,研究最佳的PBDEs的GC-MS-MS仪器分离条件及定性定量条件;对所建立的方法的回收率、检测限、重现性、精密度等参数进行考察,以建立一整套灵敏、可靠的PBDEs的GC-MS-MS分析方法。On this paper,a gas chromatooraphy tandem mass spectrometry(GC-MS-MS)method for the analysis of polybrominated diphenyl ethers(PBDEs)was established,and the optimal separation conditions,qualitative and quantitative conditions of PBDEs were studied.The recovery,detection limit,reproducibility,precision and othes parameters of tie established method were investigated to establish a set of sensitive and reliable GC-MS-MS analysis method for PBDEs.

关 键 词：多溴联苯醚 气相质谱/串联质谱 离子源温度 电子能量 碰撞能量 

分 类 号：X85[环境科学与工程—环境工程]