艾叶超临界CO2萃取浸膏GC-MS分析  

GC-MS Analysis of the Supercritical CO Extract of Artemisia Argyi

作　　者：段迪 邹颖 黄永 黄健平 熊景贤 李杰 黄建香 林泽斌 周春晖 李静[1] 邓毛程[1] Duan Di;Zou Ying;Huang Yong;Huang Jianping;Xiong Jingxian;Li Jie;Huang Jianxiang;Lin Zebin;Zhou Chunhui;Li Jing;Deng Maocheng(Guangdong Industry Technical College,Guangzhou 510300;Guangdong Geeching Biomedical Technology Co.,Ltd.,Huizhou 516081;Kangxiang Lingnan Medica Agricultural Technology Co.,Ltd.,Huizhou 5161001,China)

机构地区：[1]广东轻工职业技术学院,广东广州510300 [2]广东暨晴生物医药科技有限公司,广东惠州516081 [3]博罗县康祥岭南本草农业科技有限公司,广东惠州516100

出　　处：《广东化工》2021年第7期174-176,157,共4页Guangdong Chemical Industry

基　　金：广东省教育厅青年创新人才项目(2019GKQNCX057);广东省普通高校特色创新类项目(2018GKTSCX034,2019GKTSCX011);广东轻工职业技术学院人才类项目(KYRC2019-008);广东轻工职业技术学院领军拔尖计划项目(KYRC2019-002);广东轻工职业技术学院珠江学者人才项目(KYRC2017-001);广东轻工职业技术学院创新创业精致育人项目(2020JZYR010);广东省科技创新战略专项资金项目(“攀登计划”专项资金项目)(pdjh2021b0721)。

摘　　要：采用GC-MS法对超临界CO2萃取艾叶浸膏的化学成分进行分析,并通过面积归一化法测定各组分的相对百分含量,外标法定量研究挥发油中桉油精、樟脑、龙脑、β-石竹烯、氧化石竹烯五种标志性挥发油成分的含量。结果表明,艾叶浸膏中三十六烷(17.50%),乙酸环阿屯酯(9.38%),β-香树脂酮(8.94%),乙酸羽扇豆酯(6.01%),十八烷-9,12,15-三烯酸(3.86%)等含量比较高。桉油精、樟脑、龙脑的含量随超临界CO2萃取压力的升高而升高,β-石竹烯、氧化石竹烯含量随超临界CO2萃取压力的升高反而降低。GC-MS method was used to analyze the components of Artemisia argyi extract. Relative percentage of the components was determined by area normalization. Contents of cineole eucalyptol, camphor, borneol, β-caryophyllene and caryophyllene oxide was calculated according to the external standard method. The main compounds of Artemisia argyi extract were hexatriacontane(17.50 %), cycloartenol 3-acetate(9.38 %), β-Amyrone(8.94 %), lupeol acetate(6.01 %) and 9, 12, 15-Octadecatrienoic acid(3.86 %). The contents of eucalyptus oil, camphor and borneol increased with the increase of supercritical CO2 extraction pressure, while the contents of β-caryophylene and caryophylene oxides decreased with the increase of supercritical CO2 extraction pressure.

关 键 词：艾叶 浸膏 超临界CO2萃取 GC-MS 

分 类 号：TQ[化学工程]