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作 者:Dong Wu Shitong Wei Shanping Lu
机构地区:[1]CAS Key Laboratory of Nuclear Materials and Safety Assessment,Institute of Metal Research,Chinese Academy of Sciences,Shenyang,110016,China [2]Shenyang National Laboratory for Materials Science,Institute of Metal Research,Chinese Academy of Sciences,Shenyang,110016,China
出 处:《Acta Metallurgica Sinica(English Letters)》2021年第5期628-638,共11页金属学报(英文版)
基 金:supported by the China National Nuclear Corporation-Chinese Academy of Sciences Joint Key Laboratory of Nuclear Material and Safety Assessment。
摘 要:A 12%Cr ferritic/martensitic steel,HT-9,has been used as a primary core material for nuclear reactors.The microstructure and mechanical properties of gas tungsten arc butt welded joints of HT-9 in as-welded,and as-tempered conditions have been explored.In as-welded condition,the fusion zone(FZ)contained a fresh martensite matrix with delta(δ)-ferrite.Theδ-ferrite was rich in Cr and depleted in C compared with the matrix.The heat-aff ected zone(HAZ)could be divided into three areas as the distance from the fusion line increased:δ-ferrite/martensite duplex zone,fully recrystallized zone,and partly recrystallized zone.Prior austenitic grains did not coarsen in theδ-ferrite/martensite duplex zone due to the newly nucleatedδ-ferrite grains and incompletely ferritizing(δ-ferrite)during the welding thermal cycle.The weldment microhardness distributed heterogeneously with values above 600 HV_(1.0)in the HAZ and FZ and 250 HV_(1.0)in the base metal(BM).Solute C in the matrix,induced by the dissolution of carbide during the welding process,dominated the microhardness variation.Low toughness was observed in the FZ with a quasi-cleavage fracture tested from-80 to 20℃.The tensile fracture occurred in the relatively soft BM tested from 20 to 600℃.In as-tempered condition(760℃for 1 h),M_(23)C_6-type carbides precipitated within the martensitic laths,the lath boundaries,and theδ-ferrite/martensite interfaces.Moreover,V,Cr,Mo-rich nitrides with very small size also precipitated in theδ-ferrite/martensite interface.The tempering treatment improved the homogenous distribution of weldment hardness significantly.Tensile fracture still occurred in the BM of the weldment specimens tested from 20 to 600℃.The impact toughness improved significantly,but the ductile–brittle transaction temperature was-12℃which was higher than that of the normalized and tempered(N&T)BM.δ-ferrite was considered to be one of the major factors aggravating the impact toughness in the FZ.
关 键 词:Martensitic stainless steel Gas tungsten arc welding(GTAW) Post-weld heat treatment MICROSTRUCTURE Mechanical properties
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