新疆阿勒泰阿魏根挥发油化学成分GC-MS分析  

GC-MS Analysis of Volatile Oil of Ferula roots from Xinjiang Altay

作　　者：祖丽菲亚·吾斯曼 乃比·艾比布拉 玛依努尔·玉努斯 苏巴提·赛买提 买吾拉尼江·依孜布拉 Zulifeiya·Wusiman;Naibi·Aibibula;Mayinuer·Yunusi;Subati·Saimaiti;Maiwulanijiang·Yizibula(College of Pharmacology,Xinjiang Medical University,Urumqi 830011;The Fifth Afiliated Hospital,Xinjiang Medical University,Urumqi 830011;Central Laboratory,Xinjiang Medical University,Urumqi 830011,China)

机构地区：[1]新疆医科大学药学院,新疆乌鲁木齐830011 [2]新疆医科大学第五附属医院,新疆乌鲁木齐830011 [3]新疆医科大学中心实验室,新疆乌鲁木齐830011

出　　处：《广东化工》2021年第19期177-178,165,共3页Guangdong Chemical Industry

基　　金：大学生创新创业训练计划项目(202010760002X);新疆维吾尔自治区高校科研计划自然科学青年项目(XJEDU2017S024)。

摘　　要：目的:分析新疆阿勒泰阿魏根挥发油化学成分及相对含量。方法:利用水蒸气蒸馏法提取阿勒泰阿魏根挥发油成分,运用气相色谱-质谱联用技术(GC-MS)对挥发油进行检测,结合计算机质谱图库检索技术对分离的化合物进行结构鉴定和分析。结果:共分离鉴定了18种成分,占挥发性物质含量的99.99%。采用峰面积归一化法确定各成分的相对含量。结论:新疆阿勒泰阿魏根挥发油化学成分主要有:愈创木奠醇(44.16%)、D-柠檬烯(23.85%)、反式-橙花叔醇(7.46%)、左旋乙酸冰片酯(3.709%)、(E)-beta-金合欢烯(3.602%)等。Objective:to study the chemical composition of volatile oil of Ferula roots from Xinjiang Altay.Methods:gas chromatography-mass spectrometry(GC-MS)techniques was used to analyze the chemical composition of volatile oil of Ferula roots from Xinjiang Altay.And,the structures of the isolated compounds were identified and analyzed by computer mass spectrometry date bases retrieval technology.Results:there are 18 components separated and identified from volatile oil of Ferula roots from Xinjiang Altay by steam distillation,the amount of the identified components account for 99.99%.Conclusions:the chemical composition of volatile oil of Ferula roots from Xinjiang Altay is complex,the main components include:guaiac Dien alcohol(44.16%),limonene(23.85%),trans-Nerolidol(7.46%),L-bornyl acetate(3.709%),(E)-beta-farnesene(3.602%).

关 键 词：新疆阿勒泰 阿魏根 挥发油 气相色谱-质谱法 水蒸气蒸馏法 

分 类 号：TQ[化学工程]