微纳粉体样品库高通量并行合成的研究进展  

Research Progress on High Throughput Parallel Synthesis of Micro-nano Powders Libraries

作　　者：刘茜[1,2] 王家成 周真真[1] 徐小科 LIU Qian;WANG Jiacheng;ZHOU Zhenzhen;XU Xiaoke(The State Key Laboratory of High Performance Ceramics and Superfine Microstructure,Shanghai Institute of Ceramics,Chinese Academy of Sciences,Shanghai 200050,China;Center of Materials Science and Optoelectronics Engineering,University of Chinese Academy of Sciences,Beijing 100049,China)

机构地区：[1]中国科学院上海硅酸盐研究所,高性能陶瓷和超微结构国家重点实验室,上海200050 [2]中国科学院大学材料科学与光电子工程中心,北京100049

出　　处：《无机材料学报》2021年第12期1237-1246,共10页Journal of Inorganic Materials

基　　金：国家重点研发计划项目(2016YFB0700200,2017YFB0703200)。

摘　　要：高通量制备可通过并行合成策略快速获得大量成分准连续或梯度变化的样品,从中筛选出具有最佳成分与性能的目标材料,将传统的“试错法”研发模式变革为系统寻优的新模式,可以显著提高研发效率。高通量制备实验还可与材料计算和机器学习等虚拟实验相辅相成,验证计算结果,并为数据挖掘和应用提供更丰富的实验基础。本文综述了微纳粉体样品库高通量并行合成方法和进展,这些典型的高通量制备方法为功能粉体材料研发工作者加速实验进程提供了新思路和高效合成路径,已应用于催化剂、荧光粉、红外辐射材料、电催化材料等的快速发现和优选,并将不断扩大应用领域和规模,凸显其先进性和应用价值。The high-throughput preparation of material library can quickly obtain a large number of samples with quasi-continuous or gradient change of composition by parallel synthesis strategy,and screen the target materials with the best composition and performance.The traditional“trial and error”mode has been transformed into a new mode of system optimization in materials exploration.At the same time,high-throughput preparation experiments can complement virtual experiments such as material computing and machine learning to verify the calculation results,and provide an abundant experimental database for data mining and application.This paper reviews the parallel synthesis methods of micro-nano powder and their progress,which provide new ideas and efficient synthesis routes for the functional materials scientists to accelerate the experimental process.The mentioned high-throughput experimental methods have been applied to the rapid discovery,optimization and performance improvement of new materials,such as catalysts,phosphors,and infrared irradiative materials,which are expected to expand the application area and scale,highlighting its advancement and value.

关 键 词：并行合成 高通量 微纳粉体 阵列样品库 前驱物输运 综述 

分 类 号：TQ050[化学工程]