筋伤凝胶剂的同板多成分薄层色谱鉴别研究  

Identification of Multicomponent on One Plate of Tendon Injury Gel by TLC

作　　者：马善治[1] 潘传波[1] 郭定彬 漆伟[1] 刘才英[1] 袁海洲 谢辉[1] 彭文忠[1] Ma Shanzhi;Pan Chuanbo;Guo Dingbin;Qi Wei;Liu Caiying;Yuan Haizhou;Xie Hui;Peng Wenzhong(Chongqing Orthopaedic Hospital of Traditional Chinese Medicine,Chongqing,400012,China;Chengdu Shenghong Biotechnology Co.,Ltd.,Chengdu,611130,China)

机构地区：[1]重庆市中医骨科医院,重庆400012 [2]成都圣洪生物科技有限公司,四川成都611130

出　　处：《成都中医药大学学报》2022年第1期32-36,共5页Journal of Chengdu University of Traditional Chinese Medicine

基　　金：重庆市卫生与计划生育委员会中医药科研项目(ZY20170233)。

摘　　要：目的:针对筋伤凝胶剂处方中的主要药味大黄、没药、乳香进行同板薄层色谱鉴别,为其质量标准制定提供依据。方法:在分别对大黄、乳香、没药进行薄层鉴别的基础上,进一步优化薄层色谱鉴定方法,采用同一供试品溶液,同一展开剂同板鉴别三味药物。结果:同一薄层板上同时具有大黄、没药、乳香的鉴别特征,且阴性对照无干扰。结论:可采用同一供试品溶液,同板鉴别大黄、乳香、没药三种药物。该方法操作简便,色谱特征斑点清晰,重现性好,专属性强,可作为筋伤凝胶剂质量标准的控制依据之一。Objective:Rhei radix et rhizoma,myrth and mlibanum,which were major ingredients in prescription of Tendon Injury gel,were chosen and identified by TLC on one plate.The results provided foundation for quality control standard of the product.Methods:Based on identification results of Rhei Radix et Rhizome,myrrh,and frankincense,respectively,method for the identification was improved.The identifications were carried out on one plate with the same test solution and the same developing solvent.Results:The distinguishing characteristics of Rhei Radix et Rhizome,myrrh,and frankincense were clear.The negative control has no interference.Conclusion:It is feasible that identifying Rhei Radix et Rhizome,myrrh,and frankincense on one plate with the same test solution and the same developing solvent.The method is simple and convenient,with clear chromatographic features,good reproducibility and strong specificity.It can be used as one of the control criteria for the quality standard of Tendon Injury gel.

关 键 词：筋伤凝胶 大黄 没药 乳香 薄层色谱 

分 类 号：R284.1[医药卫生—中药学] R286.0[医药卫生—中医学]