醋乳香挥发油GC指纹图谱研究  

Study on GC Fingerprint of Volatile Oil from Vinegar Frankincense

作　　者：段雨晴 黄菊 孙婉瑾 陈树和 谢四芳 唐佩莉 段雪云 Duan Yuqing;Huang Ju;Sun Wanjin;Chen Shuhe;Xie Sifang;Tang Peili;Duan Xueyun(Hubei University of Chinese Medicine,Wuhan 430065,China;Hubei Provincial Hospital of Traditional Chinese Medicine/The Affiliated Hospital of Hubei University of Chinese Medicine/Hubei Provincial Institute of Traditional Chinese Medicine,Wuhan 430061,China)

机构地区：[1]湖北中医药大学,湖北武汉430065 [2]湖北省中医院/湖北中医药大学附属医院/湖北省中医药研究院,湖北武汉430061

出　　处：《亚太传统医药》2022年第6期61-66,共6页Asia-Pacific Traditional Medicine

基　　金：湖北省中医院院内基金:名老中医药专家涂绍川中药炮制学术思想传承及应用(ZY2019M027)。

摘　　要：目的:建立醋乳香挥发油气相色谱指纹图谱。方法:采用水蒸气蒸馏法提取醋乳香饮片中的挥发油,运用气相色谱法对10批醋乳香挥发油所含成分进行分离,得到气相色谱图,并借助“色谱指纹图谱相似度评价系统(2012A科研类)”对结果进行分析。结果:10批样品确定了20个共有峰,各样品之间的相似度在0.966~0.995之间。结论:该方法重复性良好,简便易行,可为控制和评价醋乳香饮片的内在质量提供参考。Objective:To establish the gas chromatographic fingerprint of the volatile oil of vinegar frankincense.Methods:The volatile oil in vinegar frankincense decoction pieces was extracted by steam distillation.The components contained in 10 batches of vinegar frankincense volatile oil were separated by gas chromatography to obtain the gas chromatogram,and the results were analyzed with the help of“chromatographic fingerprint similarity evaluation system(2012a scientific research class)”.Results:20 common peaks were identified in 10 batches of samples,and the similarity between each sample was 0.966~0.995.Conclusion:The method has good repeatability,is simple and feasible,and can provide reference for controlling and evaluating the internal quality of vinegar frankincense decoction pieces.

关 键 词：醋乳香 气相色谱 指纹图谱 质量控制 

分 类 号：R284.1[医药卫生—中药学]