果冻胶用冷水可溶羟丙基淀粉的制备工艺优化及应用特性研究  

Study on Preparation Process Optimization and Applicatin Characteristics of Cold Water Soluble Hydroxypropyl Starch for Jelly Glue

作　　者：吴宗帅 张淑芬 吴磊 杨公尚 张永 霍二福 程伟琴 WU Zongshuai;ZHANG Shufen;WU Lei;YANG Gongshang;ZHANG Yong;HUO Erfu;CHENG Weiqin(Henan Hengrui Technology Co.,Ltd.,Luohe 462000,China;Henan Chemical Industry Research Institute Co.,Ltd.,Zhengzhou 450052,China)

机构地区：[1]河南恒瑞淀粉科技股份有限公司,河南漯河462000 [2]河南省化工研究所有限责任公司,河南郑州450052

出　　处：《河南化工》2022年第8期21-26,共6页Henan Chemical Industry

基　　金：河南省科学院重大科研项目聚焦项目(210108004)。

摘　　要：采用响应面方法对制备冷水可溶羟丙基淀粉的条件进行了优化。通过Plackett-Burman设计筛选了制备冷水可溶羟丙基淀粉的条件,同时采用Box-Behnken设计进行了优化。结果表明:环氧丙烷用量、醚化温度、乙醇浓度和加碱量4个因素能够显著影响羟丙基含量,Box-Behnken设计预测模型显著(P<0.05),失拟项不显著(P>0.05)。用该模型预测得到的羟丙基含量为15.39%,最佳反应条件为环氧丙烷添加量19%、醚化温度43℃、乙醇浓度55%、加碱量1.8%。在最优条件下制备的羟丙基淀粉透明度、冻融稳定性、抗老化性好,用于果冻胶中,能赋予产品良好的透明度、韧性、黏结力,为果冻胶提供了新原料。Response surface methodology is used to optimize the reaction conditions for water soluble hydroxypropyl starch preparation.Plackett-Burman design is used to select reaction conditions for water soluble hydroxypropyl starch preparation,and the significant factors are optimized by Box-Behnken design.The results show that amount of propylene oxide dosage,etherification temperature,ethanol concentration and alkali addition can significantly affect the content of hydroxypropyl.The Box-Behnken model of design is significant(P<0.05),and lack of fit is no significant(P>0.05).The predicted content of the hydroxypropoxy group is 15.39%,and the predicted conditions are amount of propylene oxide 19%,etherification temperature is 43℃,ethanol concentration is 55%,amount of alkali addition is 1.8%.Properties of luminosity,the freeze thaw stability and inhibit retrogradation of hydroxypropyl starch are good under the optimal conditions.It is used in jelly,can give the product good transparency,toughness,adhesion,it provides a new raw material for jelly.

关 键 词：冷水可溶羟丙基淀粉 PLACKETT-BURMAN 因素筛选 BOX-BEHNKEN设计 果冻胶 

分 类 号：TQ433[化学工程]