Dielectric spectroscopy and structural characterization of nano-filler-loaded epoxy resin  

作　　者：S.G.Thakor V.A.Rana H.P.Vankar T.R.Pandit 

机构地区：[1]Department of Physics,School of Sciences,Gujarat University Ahmedabad 380009,Gujarat,India

出　　处：《Journal of Advanced Dielectrics》2021年第2期15-26,共12页先进电介质学报（英文）

基　　金：Authors are thankful to the funding agency DST,New Delhi for providing financial assistance,through the DST-FIST Projects(SR/FST/PSI-001/2006 and SR/FST/PSI-198/2014);Funding provided by UGC,New Delhi through DRSSAP Program Grants[Nos.F.530/10/DRS/2010(SAP-1)and F.530/17/DRS-II/2018(SAP-1)]is also gratefully acknowledged.Authors are also thankful to Prof.P.N.Gajjar,Head,Department of Physics,University School of Sciences,Gujarat University,Ahmedabad for his constant encouragement.

摘　　要：This work outlines the characterization of epoxy resin[Bisphenol A-(epichlorhydrin):epoxy]and hardener[N(3-dimethylaminopropyl)-1,3-propylenediamine]with various inorganic nano-fillers.Dielectric characterizations of epoxy,hardener,neat epoxy(epoxy+hardener)and nano-epoxy(nano-filler+neat epoxy)composites loaded with 1 wt.%of inorganic nano-fillers(SiO_(2),Al_(2)O_(3),TiO_(2)and ZnO)were carried out using precision LCR meter,over the frequency range of 1 kHz-2 MHz at a constant temperature of 300.15 K.The structural information of nano-fillers,neat epoxy and nano-epoxy composites was understood by Fourier transform infrared spectroscopy and by XRD.Moreover,hardness and shear strength(shear punch)were also determined in order to gain additional information about the mechanical properties of epoxy composite.Influence of inorganic nano-fillers on the dielectric properties,structural chemistry and mechanical properties of neat epoxy composite is discussed thoroughly in this study.

关 键 词：Epoxy resin nano-fillers dielectric relaxation spectroscopy FTIR mechanical properties XRD 

分 类 号：TB3[一般工业技术—材料科学与工程]