3,5-二溴-4-氨基-N-丁基邻苯二甲酰亚胺的制备  

Preparation of 3,5-Dibromo-4-amino-N-butylphthalimide

作　　者：丁兴成 高立江 宋龙锋 章文刚 陈海滨 何江伟 DING Xing-cheng;GAO Li-jiang;SONG Long-feng;ZHANG Wen-gang;CHEN Hai-bin;HE Jang-wei(Zhejiang Runtu Co.,Ltd.,Shaoxing 312369,Zhejiang China)

机构地区：[1]浙江闰土股份有限公司,绍兴312369

出　　处：《染料与染色》2022年第5期41-43,共3页Dyestuffs and Coloration

基　　金：浙江省万人计划科技创新领军人才资助项目(2019R52058)。

摘　　要：本文介绍了一种3,5-二溴-4-氨基-N-丁基邻苯二甲酰亚胺的合成方法。以4-氨基-N-丁基邻苯二甲酰亚胺为原料,通过溴化法合成3,5-二溴-4-氨基-N-丁基邻苯二甲酰亚胺,并考察了不同溶剂、原料投加量、溴素及双氧水用量、反应温度及反应时间等条件对该反应的影响。A synthetic process of 3,5-dibromo-4-amino-N-butylphthalimide was introduced in this paper.Using 4-amino-N-butylphthalimide as raw material,3,5-dibromo-4-amino-N-butylphthalimide was synthesized by bromination method.The effects of different solvents,raw material dosage,bromine and hydrogen peroxide dosage,reaction temperature and reaction time on the reaction were investigated.

关 键 词：4-氨基-N-丁基邻苯二甲酰亚胺 3 5-二溴-4-氨基-N-丁基邻苯二甲酰亚胺 溴化法 

分 类 号：TQ612.4[化学工程—精细化工]