六神曲中总有机酸含量的测定  

Determination of Total Organic Acids in Liushenqu

作　　者：肖瑜 魏引平 袁小倩 Xiao Yu;Wei Liping;Yuan Xiaoqian(Baoji Food and Drug Inspection and Testing Center,Baoji 721013,China;Shaanxi Pharmaceutical and Vaccine Inspection Center Baoji Branch Center,Baoji 721013,China)

机构地区：[1]宝鸡市食品药品检验检测中心,陕西宝鸡721013 [2]陕西省药品和疫苗检查中心宝鸡分中心,陕西宝鸡721013

出　　处：《黑龙江科学》2022年第24期49-50,53,共3页Heilongjiang Science

摘　　要：为了对六神曲质量进行有效评价,收集了陕西省六神曲主要生产厂家不同月份生产的24批样品,采用电位滴定法,建立了六神曲总有机酸含量测定方法,滴定至pH 8.2为终点。结果表明,该方法重现性、稳定性好,回收率在97.37%~100.88%;总有机酸含量在0.69%~2.05%,说明此方法可用于六神曲的质量控制,为有效控制质量、提升质量标准提供了科学依据。In order to effectively evaluate Liushenqu, the study collects 24 branches of Liushenqu samples from main manufactures in different months in Shaanxi Province, adopts potentiometric titration, establishes the method for the determination of total organic acids in Liushenqu. Potentiometric titration was used to titrate to pH 8.2 as the end point. The method had good reproducibility and stability, and the recovery was 97.37%~100.88%.The content of total organic acid in 24 batches of Liushenqu was between 0.69% and 2.05%.The method can be used for the quality control of Liushenqu, to provide scientific reference for effective quality control and quality standard improvement.

关 键 词：六神曲 总有机酸 含量测定 

分 类 号：R284.1[医药卫生—中药学]