超高速激光熔覆316L涂层的组织与性能  

Microstructure and properties of extreme high speed Laser cladding 316L coating

作　　者：邹勇[1] 陈明英 王秋林[1] 张宏 ZOU Yong;CHEN Mingying;WANG Qiulin;ZHANG Hong(Chengdu Aeronautic Polytechnic,Chengdu 610100,China;Avic Chengdu Aircraft Industrial(Group)Co.,Ltd.,Chengdu 610100,China;Failure Mechanics and Engineering Disaster Prevention and Mitigation Key Laboratory of Sichuan Province,College ofArchitecture and Environment,Sichuan University,Chengdu 610065,China)

机构地区：[1]成都航空职业技术学院,四川成都610100 [2]成都飞机工业(集团)有限责任公司,四川成都610091 [3]四川大学建筑与环境学院破坏力学与工程防灾减灾四川省重点实验室,四川成都610065

出　　处：《粉末冶金工业》2023年第1期67-72,共6页Powder Metallurgy Industry

基　　金：中国博士后基金资助项目(2019M653396);四川大学博士后基金资助项目(2019SCU12056);四川大学-自贡政府战略合作支持项目(2019CDZG-4);四川大学-宜宾政府战略合作支持项目(2019CDYB-24);四川省教育厅资助项目(18ZB0058)。

摘　　要：采用超高速激光熔覆技术,在45钢轴上制备了316L涂层;利用扫描电镜(SEM)观察了涂层的显微组织,用能谱仪(EDS)和X-射线衍射(XRD)进行元素及物相分析,并测试了涂层的显微硬度和耐磨性。结果表明,超高速激光熔覆技术的光斑直径小、搭接率高,故涂层的平整度高;能量密度高(约9×10^(4)W/cm^(2)),粉末完全熔化,故涂层的致密度高;熔体的体量小,冷热转换速度快,过冷度△T大,晶粒细化明显;涂层中下部由快速凝固产生的细小枝晶以及枝晶间共晶相组成,中上部的晶粒逐渐向等轴晶粒转变;搭接分界处和熔覆层/基材界面处,两边的晶粒尺寸差异较大;激光对基材有一定的稀释作用;涂层厚度不均匀,与基材结合良好,为冶金结合;316L涂层物相由γ-Fe、Cr_(0.19)Fe_(0.7)Ni_(0.11)、Fe_(63)Mo_(37)组成;由于细晶强化和第二相强化机制,316L涂层的平均硬度(634.12HV_(0.5))是45钢基体的3.07倍;耐磨性提高了31.8%,其磨损的机制主要为磨粒磨损。Using extreme high speed laser cladding technology,316L coating was prepared on 45 steel shaft.The mi‐crostructure of the coating was observed by scanning electron microscope(SEM),elemental and phase analyses were carried out by energy dispersive spectroscopy(EDS)and X-ray diffraction(XRD),the microhardness and wear resis‐tance of the coating were tested.The results show that the extreme high speed laser cladding technology has a small spot diameter and a high overlap rate,so the flatness of the coating is high.The energy density is high(about 9×10^(4)W/cm^(2)),and the powder is completely melted,so the coating has a high density.The volume of the melt is small,the heat and cold conversion speed is fast,the degree of undercoolingΔT is large,so the grain refinement is obvious.The middle and lower parts of the coating are composed of small dendrites produced by rapid solidification and inter‐dendritic eutectic phases,the middle and upper parts grains gradually transform to equiaxed grains.At the overlap boundary and at the cladding layer/substrate interface,there is a large difference in grain size on both sides.The laser has a certain dilution effect on the substrate.The coating thickness is uneven,but it is well metallurgical bonded with the base material.The phase of the 316L coating is composed ofγ-Fe,Cr_(0.19)Fe_(0.7)Ni_(0.11),Fe_(63)Mo_(37).Due to fine grain strengthening and second phase strengthening mechanism,the average hardness of the 316L coating(634.12HV_(0.5))is 3.07 times that of the 45 steel substrate.The wear resistance is increased by 31.8%,and the main wear mechanism is abrasive wear.

关 键 词：超高速激光熔覆 316L涂层 宏观形貌 显微组织 物相 硬度 耐磨性 

分 类 号：TG178[金属学及工艺—金属表面处理] TG665[金属学及工艺—金属学]